N-phenylacetoxybenzyloxycarbonyl-L-phenylalanyl-L-seryl-L-alanine allyl ester

Base Information

Chemical Name:N-phenylacetoxybenzyloxycarbonyl-L-phenylalanyl-L-seryl-L-alanine allyl ester
CAS No.:333362-87-1
Molecular Formula:C₃₄H₃₇N₃O₉
Molecular Weight:631.682
Hs Code.:

Synonyms:N-phenylacetoxybenzyloxycarbonyl-L-phenylalanyl-L-seryl-L-alanine allyl ester

Suppliers and Price of N-phenylacetoxybenzyloxycarbonyl-L-phenylalanyl-L-seryl-L-alanine allyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of N-phenylacetoxybenzyloxycarbonyl-L-phenylalanyl-L-seryl-L-alanine allyl ester

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of N-phenylacetoxybenzyloxycarbonyl-L-phenylalanyl-L-seryl-L-alanine allyl ester

There total 1 articles about N-phenylacetoxybenzyloxycarbonyl-L-phenylalanyl-L-seryl-L-alanine allyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 192999-60-3
4-(phenylacetoxy)benzyl-L-phenylalanine

: L-seryl-L-alanine allyl ester hydrotrifluoroacetate

: 333362-87-1
N-phenylacetoxybenzyloxycarbonyl-L-phenylalanyl-L-seryl-L-alanine allyl ester

Guidance literature:: With N-ethyl-N,N-diisopropylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; In N,N-dimethyl-formamide; at 0 ℃; for 1h;
DOI:10.1002/1521-3765(20020415)8:8<1879::AID-CHEM1879>3.0.CO;2-5

Reference yield:

: 108554-72-9
(allyloxy)bis(diisopropylamino)phosphine

: 333362-87-1
N-phenylacetoxybenzyloxycarbonyl-L-phenylalanyl-L-seryl-L-alanine allyl ester

: (S)-2-{(S)-3-(Allyloxy-diisopropylamino-phosphanyloxy)-2-[(S)-3-phenyl-2-(4-phenylacetoxy-benzyloxycarbonylamino)-propionylamino]-propionylamino}-propionic acid allyl ester

Guidance literature:: With 1H-tetrazole; diisopropylamine; In dichloromethane; at 0 ℃; for 1h;
DOI:10.1002/1521-3765(20020415)8:8<1879::AID-CHEM1879>3.0.CO;2-5

Reference yield:

: 333362-87-1
N-phenylacetoxybenzyloxycarbonyl-L-phenylalanyl-L-seryl-L-alanine allyl ester

: 333362-92-8
L-phenylalanyl-L-seryl-O-(3'-O-acetyl-6-N-allyloxycarbonyl-2'-deoxycytidyl-allyl-phosphato)-L-alanine allyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: (iPr)2NH; tetrazole / CH₂Cl₂ / 1 h / 0 °C

2: terazole / acetonitrile; CH₂Cl₂ / 24 h / 20 °C

3: t-BuOOH / acetonitrile; CH₂Cl₂ / 0.17 h / 0 °C

4: 69 percent / penicillin G acylase; aq. KI / aq. phosphate buffer; methanol / 24 h / 20 °C / pH 6.8

With 1H-tetrazole; tert.-butylhydroperoxide; penicillin G acylase; terazole; diisopropylamine; potassium iodide; In methanol; phosphate buffer; dichloromethane; acetonitrile;
DOI:10.1002/1521-3765(20020415)8:8<1879::AID-CHEM1879>3.0.CO;2-5