allyl 2-azido-3,6-di-O-benzyl-2-deoxy-4-O-(4-methoxybenzyl)-α-D-glucopyranoside

Base Information

Chemical Name:allyl 2-azido-3,6-di-O-benzyl-2-deoxy-4-O-(4-methoxybenzyl)-α-D-glucopyranoside
CAS No.:1215016-47-9
Molecular Formula:C₃₁H₃₅N₃O₆
Molecular Weight:545.635
Hs Code.:

Synonyms:allyl 2-azido-3,6-di-O-benzyl-2-deoxy-4-O-(4-methoxybenzyl)-α-D-glucopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of allyl 2-azido-3,6-di-O-benzyl-2-deoxy-4-O-(4-methoxybenzyl)-α-D-glucopyranoside

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Technology Process of allyl 2-azido-3,6-di-O-benzyl-2-deoxy-4-O-(4-methoxybenzyl)-α-D-glucopyranoside

There total 3 articles about allyl 2-azido-3,6-di-O-benzyl-2-deoxy-4-O-(4-methoxybenzyl)-α-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 824-94-2
p-methoxybenzyl chloride

: 628280-91-1
allyl 2-azido-3,6-di-O-benzyl-2-deoxy-α-D-glucopyranoside

: 1215016-47-9
allyl 2-azido-3,6-di-O-benzyl-2-deoxy-4-O-(4-methoxybenzyl)-α-D-glucopyranoside

Guidance literature:: With sodium hydride; In N,N-dimethyl-formamide; at 0 ℃;
DOI:10.1016/j.tetlet.2009.12.124

Reference yield: 80.0%

: 1450734-54-9
4-methoxybenzyl N-phenyl-2,2,2-trifluoroacetimidate

: 628280-91-1
allyl 2-azido-3,6-di-O-benzyl-2-deoxy-α-D-glucopyranoside

: 1215016-47-9
allyl 2-azido-3,6-di-O-benzyl-2-deoxy-4-O-(4-methoxybenzyl)-α-D-glucopyranoside

Guidance literature:: With bismuth(lll) trifluoromethanesulfonate; In toluene; at 20 ℃; for 24h; regioselective reaction; Molecular sieve; Inert atmosphere;
DOI:10.1016/j.tetlet.2013.07.066

Reference yield:

: 105-13-5
4-Methoxybenzyl alcohol

: 1215016-47-9
allyl 2-azido-3,6-di-O-benzyl-2-deoxy-4-O-(4-methoxybenzyl)-α-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydride / dichloromethane; mineral oil / 2 h / 0 - 20 °C / Inert atmosphere

2: bismuth(lll) trifluoromethanesulfonate / toluene / 24 h / 20 °C / Molecular sieve; Inert atmosphere

With bismuth(lll) trifluoromethanesulfonate; sodium hydride; In dichloromethane; toluene; mineral oil;
DOI:10.1016/j.tetlet.2013.07.066