N-[1-(4-chlorobenzoylamino)-2,2-dichloroethyl]-4-chlorobenzamide

Base Information

• Chemical Name: N-[1-(4-chlorobenzoylamino)-2,2-dichloroethyl]-4-chlorobenzamide
• CAS No.: 130775-07-4
• Molecular Formula: C₁₆H₁₂Cl₄N₂O₂
• Molecular Weight: 406.095
• Mol file: 130775-07-4.mol

Synonyms:N-[1-(4-chlorobenzoylamino)-2,2-dichloroethyl]-4-chlorobenzamide

Chemical Property of N-[1-(4-chlorobenzoylamino)-2,2-dichloroethyl]-4-chlorobenzamide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N-[1-(4-chlorobenzoylamino)-2,2-dichloroethyl]-4-chlorobenzamide

There total 1 articles about N-[1-(4-chlorobenzoylamino)-2,2-dichloroethyl]-4-chlorobenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

N-(1-Amino-2,2-dichloro-ethyl)-4-chloro-benzamide (90283-57-1) + 4-chloro-benzoyl chloride (122-01-0) → N-[1-(4-chlorobenzoylamino)-2,2-dichloroethyl]-4-chlorobenzamide (130775-07-4)

Guidance literature:

With triethylamine; In benzene; at 20 - 25 ℃; for 24h;

Reference yield: 63.0%

N-[1-(4-chlorobenzoylamino)-2,2-dichloroethyl]-4-chlorobenzamide (130775-07-4) → 2,5-bis(4-chlorophenyl)-3a,6a-dihydro[1,3]thiazolo[4,5-d][1,3]thiazole (1206128-28-0)

Guidance literature:

With Lawessons reagent; In 1,4-dioxane; Reflux;

DOI:10.1002/hc.20493

Reference yield: 56.0%

N-[1-(4-chlorobenzoylamino)-2,2-dichloroethyl]-4-chlorobenzamide (130775-07-4) → 4-Chloro-N-[2-(4-chloro-phenyl)-oxazol-4-yl]-benzamide (130775-29-0)

Guidance literature:

With sodium methylate; In tetrahydrofuran; methanol; at 20 - 25 ℃; for 168h;

upstream raw materials:

N-(1-Amino-2,2-dichloro-ethyl)-4-chloro-benzamide

4-chloro-benzoyl chloride

Downstream raw materials:

4-Chloro-N-[2-(4-chloro-phenyl)-oxazol-4-yl]-benzamide

2,5-bis(4-chlorophenyl)-3a,6a-dihydro[1,3]thiazolo[4,5-d][1,3]thiazole