(R)-4-(3-(2-allyloxyethyl)-2-benzyloxy-1-naphthyl)-3-benzyloxy-2-naphthaleneacetaldehyde

Base Information

Chemical Name:(R)-4-(3-(2-allyloxyethyl)-2-benzyloxy-1-naphthyl)-3-benzyloxy-2-naphthaleneacetaldehyde
CAS No.:350490-38-9
Molecular Formula:C₄₁H₃₆O₄
Molecular Weight:592.734
Hs Code.:

Synonyms:(R)-4-(3-(2-allyloxyethyl)-2-benzyloxy-1-naphthyl)-3-benzyloxy-2-naphthaleneacetaldehyde

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Chemical Property of (R)-4-(3-(2-allyloxyethyl)-2-benzyloxy-1-naphthyl)-3-benzyloxy-2-naphthaleneacetaldehyde

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Technology Process of (R)-4-(3-(2-allyloxyethyl)-2-benzyloxy-1-naphthyl)-3-benzyloxy-2-naphthaleneacetaldehyde

There total 3 articles about (R)-4-(3-(2-allyloxyethyl)-2-benzyloxy-1-naphthyl)-3-benzyloxy-2-naphthaleneacetaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 350490-37-8
(R)-4-(3-(2-allyloxyethyl)-2-benzyloxy-1-naphthyl)-3-benzyloxy-2-naphthaleneethanol

: 350490-38-9
(R)-4-(3-(2-allyloxyethyl)-2-benzyloxy-1-naphthyl)-3-benzyloxy-2-naphthaleneacetaldehyde

Guidance literature:: With Dess-Martin periodane; In dichloromethane; at 0 - 20 ℃; for 2h;
DOI:10.1016/S0040-4020(01)00070-9

Reference yield:

: 173961-77-8,350490-35-6,211560-94-0
(R)-3,3'-bis(2-hydroxyethyl)-2,2'-bis(methoxymethyloxy)-1,1'-binaphthyl

: 350490-38-9
(R)-4-(3-(2-allyloxyethyl)-2-benzyloxy-1-naphthyl)-3-benzyloxy-2-naphthaleneacetaldehyde

Guidance literature:: Multi-step reaction with 3 steps

1.1: 48 percent / KF-alumina / acetonitrile / 20 h / 20 °C

2.1: TsOH*H₂O / CH₂Cl₂; methanol / 6.5 h / 20 °C

2.2: 73 percent / NaH / tetrahydrofuran; dimethylformamide / 3.5 h / 0 - 20 °C

3.1: 77 percent / Dess-Martin periodinate / CH₂Cl₂ / 2 h / 0 - 20 °C

With potassium fluoride on basic alumina; Dess-Martin periodane; toluene-4-sulfonic acid; In methanol; dichloromethane; acetonitrile;
DOI:10.1016/S0040-4020(01)00070-9

Reference yield:

: 350490-36-7
(R)-4-(3-(2-allyloxyethyl)-2-methoxymethyloxy-1-naphthyl)-3-methoxymethyloxy-2-naphthaleneethanol

: 350490-38-9
(R)-4-(3-(2-allyloxyethyl)-2-benzyloxy-1-naphthyl)-3-benzyloxy-2-naphthaleneacetaldehyde

Guidance literature:: Multi-step reaction with 2 steps

1.1: TsOH*H₂O / CH₂Cl₂; methanol / 6.5 h / 20 °C

1.2: 73 percent / NaH / tetrahydrofuran; dimethylformamide / 3.5 h / 0 - 20 °C

2.1: 77 percent / Dess-Martin periodinate / CH₂Cl₂ / 2 h / 0 - 20 °C

With Dess-Martin periodane; toluene-4-sulfonic acid; In methanol; dichloromethane;
DOI:10.1016/S0040-4020(01)00070-9