(R)-4-(3-(2-allyloxyethyl)-2-benzyloxy-1-naphthyl)-3-benzyloxy-2-naphthaleneethanol

Base Information

Chemical Name:(R)-4-(3-(2-allyloxyethyl)-2-benzyloxy-1-naphthyl)-3-benzyloxy-2-naphthaleneethanol
CAS No.:350490-37-8
Molecular Formula:C₄₁H₃₈O₄
Molecular Weight:594.75
Hs Code.:

Synonyms:(R)-4-(3-(2-allyloxyethyl)-2-benzyloxy-1-naphthyl)-3-benzyloxy-2-naphthaleneethanol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (R)-4-(3-(2-allyloxyethyl)-2-benzyloxy-1-naphthyl)-3-benzyloxy-2-naphthaleneethanol

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Technology Process of (R)-4-(3-(2-allyloxyethyl)-2-benzyloxy-1-naphthyl)-3-benzyloxy-2-naphthaleneethanol

There total 3 articles about (R)-4-(3-(2-allyloxyethyl)-2-benzyloxy-1-naphthyl)-3-benzyloxy-2-naphthaleneethanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 100-39-0
benzyl bromide

: 350490-36-7
(R)-4-(3-(2-allyloxyethyl)-2-methoxymethyloxy-1-naphthyl)-3-methoxymethyloxy-2-naphthaleneethanol

: 350490-37-8
(R)-4-(3-(2-allyloxyethyl)-2-benzyloxy-1-naphthyl)-3-benzyloxy-2-naphthaleneethanol

Guidance literature:: (R)-4-(3-(2-allyloxyethyl)-2-methoxymethyloxy-1-naphthyl)-3-methoxymethyloxy-2-naphthaleneethanol; With toluene-4-sulfonic acid; In methanol; dichloromethane; at 20 ℃; for 6.5h;

benzyl bromide; With sodium hydride; In tetrahydrofuran; N,N-dimethyl-formamide; at 0 - 20 ℃; for 3.5h;
DOI:10.1016/S0040-4020(01)00070-9

Reference yield:

: 350490-38-9
(R)-4-(3-(2-allyloxyethyl)-2-benzyloxy-1-naphthyl)-3-benzyloxy-2-naphthaleneacetaldehyde

: 350490-37-8
(R)-4-(3-(2-allyloxyethyl)-2-benzyloxy-1-naphthyl)-3-benzyloxy-2-naphthaleneethanol

: C₈₂H₇₄O₇

Guidance literature:: With triethylsilane; trimethylsilyl trifluoromethanesulfonate; In dichloromethane; at 0 ℃; for 1h;
DOI:10.1016/S0040-4020(01)00070-9

Reference yield:

: 173961-77-8,350490-35-6,211560-94-0
(R)-3,3'-bis(2-hydroxyethyl)-2,2'-bis(methoxymethyloxy)-1,1'-binaphthyl

: 350490-37-8
(R)-4-(3-(2-allyloxyethyl)-2-benzyloxy-1-naphthyl)-3-benzyloxy-2-naphthaleneethanol

Guidance literature:: Multi-step reaction with 2 steps

1.1: 48 percent / KF-alumina / acetonitrile / 20 h / 20 °C

2.1: TsOH*H₂O / CH₂Cl₂; methanol / 6.5 h / 20 °C

2.2: 73 percent / NaH / tetrahydrofuran; dimethylformamide / 3.5 h / 0 - 20 °C

With potassium fluoride on basic alumina; toluene-4-sulfonic acid; In methanol; dichloromethane; acetonitrile;
DOI:10.1016/S0040-4020(01)00070-9