(4S,5S)-N-(tert-butyloxycarbonyl)-5-ethenyl-4-phenylmethyl oxazolidin-2-one

Base Information

Chemical Name:(4S,5S)-N-(tert-butyloxycarbonyl)-5-ethenyl-4-phenylmethyl oxazolidin-2-one
CAS No.:265996-32-5
Molecular Formula:C₁₇H₂₁NO₄
Molecular Weight:303.358
Hs Code.:

Synonyms:(4S,5S)-N-(tert-butyloxycarbonyl)-5-ethenyl-4-phenylmethyl oxazolidin-2-one

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Chemical Property of (4S,5S)-N-(tert-butyloxycarbonyl)-5-ethenyl-4-phenylmethyl oxazolidin-2-one

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Technology Process of (4S,5S)-N-(tert-butyloxycarbonyl)-5-ethenyl-4-phenylmethyl oxazolidin-2-one

There total 2 articles about (4S,5S)-N-(tert-butyloxycarbonyl)-5-ethenyl-4-phenylmethyl oxazolidin-2-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 24424-99-5
di-tert-butyl dicarbonate

: 99113-28-7
(3S,4S)-5-[(tert-butoxycarbonyl)amino]-3-hydroxy-5-phenyl-1-pentene

: 265996-32-5
(4S,5S)-N-(tert-butyloxycarbonyl)-5-ethenyl-4-phenylmethyl oxazolidin-2-one

Guidance literature:: (3S,4S)-5-[(tert-butoxycarbonyl)amino]-3-hydroxy-5-phenyl-1-pentene; With sodium hydride; In tetrahydrofuran; for 0.25h; Heating;

di-tert-butyl dicarbonate; In tetrahydrofuran; at 0 - 20 ℃; for 1.5h;
DOI:10.1039/b203482d

Reference yield: 45.0%

: 24424-99-5
di-tert-butyl dicarbonate

: 265996-19-8
(4S,5RS)-5-ethenyl-4-phenylmethyloxazolidin-2-one

: 229981-17-3
(4S,5R)-N-(tert-butyloxycarbonyl)-5-ethenyl-4-phenylmethyl oxazolidin-2-one

: 265996-32-5
(4S,5S)-N-(tert-butyloxycarbonyl)-5-ethenyl-4-phenylmethyl oxazolidin-2-one

Guidance literature:: With dmap; triethylamine; In tetrahydrofuran;
DOI:10.1021/ja993897c

Reference yield: 48.0%

: 64-17-5
ethanol

: 265996-32-5
(4S,5S)-N-(tert-butyloxycarbonyl)-5-ethenyl-4-phenylmethyl oxazolidin-2-one

: ethyl (3E,5S)-5-N-(tert-butyloxycarbonyl)amino-6-phenylhex-3-enoate

Guidance literature:: With carbon monoxide; bis(triphenylphosphine) palladium (Il) acetate; at 70 ℃; for 120h; under 41802.8 - 49403.3 Torr;
DOI:10.1021/ja993897c