Technology Process of 5-3-(Dimethylamino)propyl-10,11-dihydro-5H-dibenz[b, f]-azepine monohydrochloride
There total 1 articles about 5-3-(Dimethylamino)propyl-10,11-dihydro-5H-dibenz[b, f]-azepine monohydrochloride which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
In
acetone;
for 0.5h;
Heating / reflux;
In
di-isopropyl ether;
at 0 - 5 ℃;
- Guidance literature:
-
In
water;
at 20 - 62 ℃;
for 19.95h;
- Guidance literature:
-
With
peroxidase from horseradish type VI; dihydrogen peroxide;
at 37 ℃;
for 1h;
pH=7;
aq. phosphate buffer;
Enzymatic reaction;
DOI:10.1021/tx100221b