C₄₂H₆₈O₅Si₂

Base Information

Chemical Name:C₄₂H₆₈O₅Si₂
CAS No.:1207069-41-7
Molecular Formula:C₄₂H₆₈O₅Si₂
Molecular Weight:709.17
Hs Code.:

C<sub>42</sub>H<sub>68</sub>O<sub>5</sub>Si<sub>2</sub>

Synonyms:C₄₂H₆₈O₅Si₂

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Chemical Property of C₄₂H₆₈O₅Si₂

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Technology Process of C₄₂H₆₈O₅Si₂

There total 11 articles about C₄₂H₆₈O₅Si₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 1207069-55-3
C₄₂H₇₀O₅Si₂

: 1207069-41-7
C₄₂H₆₈O₅Si₂

Guidance literature:: With Dess-Martin periodane; In dichloromethane; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1021/ol902778y

Reference yield:

: 1207069-51-9
C₄₉H₇₆O₅Si₂

: 1207069-41-7
C₄₂H₆₈O₅Si₂

Guidance literature:: Multi-step reaction with 2 steps

1: 10% palladium on activated charcoal; hydrogen / ethyl acetate / 20 °C

2: Dess-Martin periodane / dichloromethane / 20 °C

With 10% palladium on activated charcoal; hydrogen; Dess-Martin periodane; In dichloromethane; ethyl acetate;
DOI:10.1002/chem.201003135

Reference yield:

: 910046-59-2
tert-butyl-[(3S)-(4-methoxybenzyloxy)hex-5-enyloxy]diphenylsilane

: 1207069-41-7
C₄₂H₆₈O₅Si₂

Guidance literature:: Multi-step reaction with 9 steps

1.1: osmium(VIII) oxide; 4-methylmorpholine N-oxide / tetrahydrofuran; water / 20 °C

1.2: 20 °C

2.1: magnesium bromide diethyl etherate / dichloromethane / 0 °C

3.1: 2,6-dimethylpyridine / dichloromethane / 0 °C

4.1: 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane; water / 20 °C / pH 7 / aq. buffer

5.1: Hoveyda-Grubbs catalyst second generation / dichloromethane / 35 °C

6.1: potassium tert-butylate / tetrahydrofuran / 0 °C

7.1: triethylsilane; boron trifluoride diethyl etherate / dichloromethane / -60 - -25 °C

8.1: 10% palladium on activated charcoal; hydrogen / ethyl acetate / 20 °C

9.1: Dess-Martin periodane / dichloromethane / 20 °C

With 2,6-dimethylpyridine; triethylsilane; osmium(VIII) oxide; Hoveyda-Grubbs catalyst second generation; magnesium bromide diethyl etherate; 10% palladium on activated charcoal; boron trifluoride diethyl etherate; potassium tert-butylate; hydrogen; Dess-Martin periodane; 4-methylmorpholine N-oxide; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In tetrahydrofuran; dichloromethane; water; ethyl acetate;
DOI:10.1002/chem.201003135