(7-Methoxy-1-phenylselanyl-indan-1-yl)-(2-phenylethynyl-phenyl)-methanone

Base Information

Chemical Name:(7-Methoxy-1-phenylselanyl-indan-1-yl)-(2-phenylethynyl-phenyl)-methanone
CAS No.:105211-13-0
Molecular Formula:C₃₁H₂₄O₂Se
Molecular Weight:507.49
Hs Code.:

Synonyms:(7-Methoxy-1-phenylselanyl-indan-1-yl)-(2-phenylethynyl-phenyl)-methanone

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Chemical Property of (7-Methoxy-1-phenylselanyl-indan-1-yl)-(2-phenylethynyl-phenyl)-methanone

Chemical Property:

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Technology Process of (7-Methoxy-1-phenylselanyl-indan-1-yl)-(2-phenylethynyl-phenyl)-methanone

There total 5 articles about (7-Methoxy-1-phenylselanyl-indan-1-yl)-(2-phenylethynyl-phenyl)-methanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 5707-04-0
Phenylselenyl chloride

: 105211-12-9
(7-Methoxy-indan-1-yl)-(2-phenylethynyl-phenyl)-methanone

: 105211-13-0
(7-Methoxy-1-phenylselanyl-indan-1-yl)-(2-phenylethynyl-phenyl)-methanone

Guidance literature:: With lithium diisopropyl amide; In tetrahydrofuran; 1.) -78 deg C, 1 h, 2.) 0 deg C, 15 min;
DOI:10.1039/c39860000878

Reference yield:

: 34985-41-6
7-methoxy-indan-1-one

: 105211-13-0
(7-Methoxy-1-phenylselanyl-indan-1-yl)-(2-phenylethynyl-phenyl)-methanone

Guidance literature:: Multi-step reaction with 5 steps

2: toluene-p-sulphonic acid / dioxane; H₂O / 14 h / Heating

3: chromic acid / acetone / 0 °C

4: 55 percent / LDA / tetrahydrofuran / 1.) -78 deg C, 1 h; 50 deg C, 1 h, 2.) -78 deg C, 20 min; 0 deg C, 20 min

5: 76 percent / LDA / tetrahydrofuran / 1.) -78 deg C, 1 h, 2.) 0 deg C, 15 min

With chromic acid; toluene-4-sulfonic acid; lithium diisopropyl amide; In tetrahydrofuran; 1,4-dioxane; water; acetone;
DOI:10.1039/c39860000878

Reference yield:

: 107135-57-9
2,3-dihydro-7-methoxy-1H-indene-1-carboxaldehyde

: 105211-13-0
(7-Methoxy-1-phenylselanyl-indan-1-yl)-(2-phenylethynyl-phenyl)-methanone

Guidance literature:: Multi-step reaction with 3 steps

1: chromic acid / acetone / 0 °C

2: 55 percent / LDA / tetrahydrofuran / 1.) -78 deg C, 1 h; 50 deg C, 1 h, 2.) -78 deg C, 20 min; 0 deg C, 20 min

3: 76 percent / LDA / tetrahydrofuran / 1.) -78 deg C, 1 h, 2.) 0 deg C, 15 min

With chromic acid; lithium diisopropyl amide; In tetrahydrofuran; acetone;
DOI:10.1039/c39860000878