benzyl hydrogen (RS)-2-benzylmalonate

Base Information

Chemical Name:benzyl hydrogen (RS)-2-benzylmalonate
CAS No.:24132-69-2
Molecular Formula:C₁₇H₁₆O₄
Molecular Weight:284.312
Hs Code.:

Synonyms:benzyl hydrogen (RS)-2-benzylmalonate

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Chemical Property of benzyl hydrogen (RS)-2-benzylmalonate

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Technology Process of benzyl hydrogen (RS)-2-benzylmalonate

There total 5 articles about benzyl hydrogen (RS)-2-benzylmalonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 3709-27-1
5-benzyl-2,2-dimethyl-1,3-dioxane-4,6-dione

: 100-51-6,185532-71-2
benzyl alcohol

: 24132-69-2
benzyl hydrogen (RS)-2-benzylmalonate

Guidance literature:: In toluene; at 70 ℃; for 12h;
DOI:10.1021/jm00356a003

Reference yield:

: 616-75-1
2-benzylmalonic acid

: 24132-69-2
benzyl hydrogen (RS)-2-benzylmalonate

Guidance literature:: Multi-step reaction with 2 steps

1: 45 percent / acetic anhydride, concd. H₂SO₄ / 1 h / Ambient temperature

2: 90 percent / toluene / 12 h / 70 °C

With sulfuric acid; acetic anhydride; In toluene;
DOI:10.1021/jm00356a003

Reference yield:

: 1214-54-6
5-benzylidene Meldrum's acid

: 24132-69-2
benzyl hydrogen (RS)-2-benzylmalonate

Guidance literature:: Multi-step reaction with 2 steps

1: sodium tris(acetoxy)borohydride / ethanol / 1 h / 20 °C / Inert atmosphere

2: toluene / 24 h / 80 °C

With sodium tris(acetoxy)borohydride; In ethanol; toluene;
DOI:10.3762/bjoc.17.135