phenacyl (R)-3-(octadecanoyloxy)icosanoate

Base Information

Chemical Name:phenacyl (R)-3-(octadecanoyloxy)icosanoate
CAS No.:828939-43-1
Molecular Formula:C₄₆H₈₀O₅
Molecular Weight:713.138
Hs Code.:

Synonyms:phenacyl (R)-3-(octadecanoyloxy)icosanoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of phenacyl (R)-3-(octadecanoyloxy)icosanoate

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Technology Process of phenacyl (R)-3-(octadecanoyloxy)icosanoate

There total 5 articles about phenacyl (R)-3-(octadecanoyloxy)icosanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 112-76-5
Stearoyl chloride

: 828939-85-1
phenacyl (R)-3-hydroxyicosanoate

: 828939-43-1
phenacyl (R)-3-(octadecanoyloxy)icosanoate

Guidance literature:: With dmap; In dichloromethane; at 20 ℃; for 3h;
DOI:10.1016/j.tet.2004.10.017

Reference yield:

: 14531-35-2
methyl 3-oxoicosanoate

: 828939-43-1
phenacyl (R)-3-(octadecanoyloxy)icosanoate

Guidance literature:: Multi-step reaction with 4 steps

1: 77 percent / hydrogen; (R)-(+)-2,2'-bis(diphenylphosphino)-1,1'-binaphthyl-RuCl₂ / methanol / 44 h / 60 °C / 64600 Torr

2: NaOH / tetrahydrofuran; H₂O / 4 h / Heating

3: 1.1 g / triethylamine / ethyl acetate / 20 h / 45 °C

4: 88 percent / DMAP / CH₂Cl₂ / 3 h / 20 °C

With dmap; sodium hydroxide; dichloro-R-2,2′-bis(diphenylphosphino)-1,1′-binaphthyl ruthenium; hydrogen; triethylamine; In tetrahydrofuran; methanol; dichloromethane; water; ethyl acetate; 1: Noyori hydrogenation;
DOI:10.1016/j.tet.2004.10.017

Reference yield:

: 136890-22-7
(R)-β-hydroxyeicosanoic acid methyl ester

: 828939-43-1
phenacyl (R)-3-(octadecanoyloxy)icosanoate

Guidance literature:: Multi-step reaction with 3 steps

1: NaOH / tetrahydrofuran; H₂O / 4 h / Heating

2: 1.1 g / triethylamine / ethyl acetate / 20 h / 45 °C

3: 88 percent / DMAP / CH₂Cl₂ / 3 h / 20 °C

With dmap; sodium hydroxide; triethylamine; In tetrahydrofuran; dichloromethane; water; ethyl acetate;
DOI:10.1016/j.tet.2004.10.017