(1R,4S)-3-[(E)-3,5-Dimethyl-phenylimino]-1,7,7-trimethyl-bicyclo[2.2.1]heptan-2-one

Base Information

• Chemical Name: (1R,4S)-3-[(E)-3,5-Dimethyl-phenylimino]-1,7,7-trimethyl-bicyclo[2.2.1]heptan-2-one
• CAS No.: 87360-00-7
• Molecular Formula: C₁₈H₂₃NO
• Molecular Weight: 269.387

Synonyms:(1R,4S)-3-[(E)-3,5-Dimethyl-phenylimino]-1,7,7-trimethyl-bicyclo[2.2.1]heptan-2-one

Chemical Property of (1R,4S)-3-[(E)-3,5-Dimethyl-phenylimino]-1,7,7-trimethyl-bicyclo[2.2.1]heptan-2-one

Chemical Property:

Purity/Quality:

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MSDS Files:

SDS file from LookChem

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Technology Process of (1R,4S)-3-[(E)-3,5-Dimethyl-phenylimino]-1,7,7-trimethyl-bicyclo[2.2.1]heptan-2-one

There total 1 articles about (1R,4S)-3-[(E)-3,5-Dimethyl-phenylimino]-1,7,7-trimethyl-bicyclo[2.2.1]heptan-2-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(R)-camphorquinone (10334-26-6) + 3,5-dimethylaminoaniline (108-69-0) → (1R,4S)-3-[(E)-3,5-Dimethyl-phenylimino]-1,7,7-trimethyl-bicyclo[2.2.1]heptan-2-one (87360-00-7)

Guidance literature:

In ethanol;

DOI:10.1016/j.jinorgbio.2019.110791

Reference yield:

(1R,4S)-3-[(E)-3,5-Dimethyl-phenylimino]-1,7,7-trimethyl-bicyclo[2.2.1]heptan-2-one (87360-00-7) + silver nitrate → C36H46AgN3O5

Guidance literature:

In acetonitrile; at 20 ℃; for 2h; Schlenk technique; Darkness; Inert atmosphere;

DOI:10.1016/j.jinorgbio.2019.110791

Reference yield:

(1R,4S)-3-[(E)-3,5-Dimethyl-phenylimino]-1,7,7-trimethyl-bicyclo[2.2.1]heptan-2-one (87360-00-7) → (1R,3S,4S)-3-(3,5-Dimethyl-phenylamino)-1,7,7-trimethyl-bicyclo[2.2.1]heptan-2-one (87360-01-8)

Guidance literature:

With potassium hydroxide; zinc; In ethanol; at 25 ℃;

DOI:10.1016/S0040-4039(00)88138-1

upstream raw materials:

(R)-camphorquinone

3,5-dimethylaminoaniline

Downstream raw materials:

(1R,3S,4S)-3-(3,5-Dimethyl-phenylamino)-1,7,7-trimethyl-bicyclo[2.2.1]heptan-2-one

(1R,2S,3R)-3-[N-Phenylsulfonyl-N-(3,5-dimethylphenyl)amino]bornan-2-ol

N-(3,5-Dimethyl-phenyl)-N-((1S,2S,3R,4R)-3-hydroxy-4,7,7-trimethyl-bicyclo[2.2.1]hept-2-yl)-benzenesulfonamide

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