(biphenyl-4-yl)-[(biphenyl-2,3,5,6-d4)-4-yl]amine

Base Information

Chemical Name:(biphenyl-4-yl)-[(biphenyl-2,3,5,6-d4)-4-yl]amine
CAS No.:1322090-85-6
Molecular Formula:C₂₄H₁₉N
Molecular Weight:325.39
Hs Code.:

Synonyms:(biphenyl-4-yl)-[(biphenyl-2,3,5,6-d4)-4-yl]amine

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Chemical Property of (biphenyl-4-yl)-[(biphenyl-2,3,5,6-d4)-4-yl]amine

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Technology Process of (biphenyl-4-yl)-[(biphenyl-2,3,5,6-d4)-4-yl]amine

There total 6 articles about (biphenyl-4-yl)-[(biphenyl-2,3,5,6-d4)-4-yl]amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.7%

: 1322090-83-4
(biphenyl-4-yl)-4-bromo(phenyl-2,3,5,6-d4)amine

: 98-80-6
phenylboronic acid

: 1322090-85-6
(biphenyl-4-yl)-[(biphenyl-2,3,5,6-d4)-4-yl]amine

Guidance literature:: With potassium phosphate; tri-tert-butyl phosphine; palladium diacetate; In tetrahydrofuran; at 60 ℃; for 12.5h; Inert atmosphere;

Reference yield:

: 4165-61-1
aniline-d5

: 1322090-85-6
(biphenyl-4-yl)-[(biphenyl-2,3,5,6-d4)-4-yl]amine

Guidance literature:: Multi-step reaction with 5 steps

1: acetic acid / 4 h / 70 °C / Inert atmosphere

2: potassium carbonate; sodium sulfite / copper / 1-dodecylbenzene / 34 h / 210 °C / Inert atmosphere

3: potassium hydroxide; water / i-Amyl alcohol / 3 h / Inert atmosphere; Reflux

4: N-Bromosuccinimide / N,N-dimethyl-formamide / 3 h / 20 °C / Inert atmosphere; Cooling with ice

5: potassium phosphate / palladium diacetate; tri-tert-butyl phosphine / tetrahydrofuran / 12.5 h / 60 °C / Inert atmosphere

With potassium phosphate; N-Bromosuccinimide; water; potassium carbonate; acetic acid; potassium hydroxide; sodium sulfite; tri-tert-butyl phosphine; palladium diacetate; copper; In tetrahydrofuran; i-Amyl alcohol; 1-dodecylbenzene; N,N-dimethyl-formamide;

Reference yield:

: 15826-91-2
acetanilide-d5

: 1322090-85-6
(biphenyl-4-yl)-[(biphenyl-2,3,5,6-d4)-4-yl]amine

Guidance literature:: Multi-step reaction with 4 steps

1: potassium carbonate; sodium sulfite / copper / 1-dodecylbenzene / 34 h / 210 °C / Inert atmosphere

2: potassium hydroxide; water / i-Amyl alcohol / 3 h / Inert atmosphere; Reflux

3: N-Bromosuccinimide / N,N-dimethyl-formamide / 3 h / 20 °C / Inert atmosphere; Cooling with ice

4: potassium phosphate / palladium diacetate; tri-tert-butyl phosphine / tetrahydrofuran / 12.5 h / 60 °C / Inert atmosphere

With potassium phosphate; N-Bromosuccinimide; water; potassium carbonate; potassium hydroxide; sodium sulfite; tri-tert-butyl phosphine; palladium diacetate; copper; In tetrahydrofuran; i-Amyl alcohol; 1-dodecylbenzene; N,N-dimethyl-formamide;