HC[(CMe)(NC₆F₅)]2AlClMe

Base Information

Chemical Name:HC[(CMe)(NC₆F₅)]2AlClMe
CAS No.:880095-67-0
Molecular Formula:C₁₈H₁₀AlClF₁₀N₂
Molecular Weight:506.709
Hs Code.:

HC[(CMe)(NC<sub>6</sub>F<sub>5</sub>)]2AlClMe

Synonyms:HC[(CMe)(NC₆F₅)]2AlClMe

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Chemical Property of HC[(CMe)(NC₆F₅)]2AlClMe

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Technology Process of HC[(CMe)(NC₆F₅)]2AlClMe

There total 1 articles about HC[(CMe)(NC₆F₅)]2AlClMe which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: HC(C(CH₃)NC₆F₅)C(CH₃)NHC₆F₅

: 917-65-7
methylaluminum dichloride

: 880095-67-0
HC[(CMe)(NC₆F₅)]2AlClMe

Guidance literature:: With n-C₄H₉Li; In toluene; byproducts: LiCl; (N2); a soln. of n-BuLi added dropwise to a soln. of ligand at 0°C, stirred and allowed to warm to room temp., stirred for 12 h, cooled to 0°C, Al compd. added, allowed to warm to room temp. and stirredfor 12 h; filtered, dried (vac.), washed (n-hexane); elem. anal.;
DOI:10.1021/ic051718o

Reference yield: 69.0%

: 880095-67-0
HC[(CMe)(NC₆F₅)]2AlClMe

: 7732-18-5
water

: 880095-71-6
(HC[(CMe)(NC6F5)]2AlMe)2(μ-O)

: HC[(CMe)(NC₆F₅)]2AlMe(OH)

Guidance literature:: With 1,3-diisopropyl-4,5-dimethylimidazol-2-ylidene; In toluene; (N2); H2O added at 0°C to a mixt. of Al complex and 1,3-diisopropyl-4,5-dimethylimidazol-2-ylidene, allowed to warm to room temp. and stirred for 12 h; filtered, dried (vac.), extd. (n-hexane), crystd. at -28°C; elem.anal.;
DOI:10.1021/ic051718o