N-bis(trimethylsilyl)methyl-N-[2-(4-methoxyphenyl)ethyl]-α-methoxycarbonyl-α-diazoacetamide

Base Information

Chemical Name:N-bis(trimethylsilyl)methyl-N-[2-(4-methoxyphenyl)ethyl]-α-methoxycarbonyl-α-diazoacetamide
CAS No.:882408-54-0
Molecular Formula:C₂₀H₃₃N₃O₄Si₂
Molecular Weight:435.671
Hs Code.:

Synonyms:N-bis(trimethylsilyl)methyl-N-[2-(4-methoxyphenyl)ethyl]-α-methoxycarbonyl-α-diazoacetamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-bis(trimethylsilyl)methyl-N-[2-(4-methoxyphenyl)ethyl]-α-methoxycarbonyl-α-diazoacetamide

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Technology Process of N-bis(trimethylsilyl)methyl-N-[2-(4-methoxyphenyl)ethyl]-α-methoxycarbonyl-α-diazoacetamide

There total 3 articles about N-bis(trimethylsilyl)methyl-N-[2-(4-methoxyphenyl)ethyl]-α-methoxycarbonyl-α-diazoacetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 882408-55-1
N-(4-methoxyphenethyl)bis(trimethylsilyl)methylamine

: 60180-61-2
methyl diazomalonyl chloride

: 882408-54-0
N-bis(trimethylsilyl)methyl-N-[2-(4-methoxyphenyl)ethyl]-α-methoxycarbonyl-α-diazoacetamide

Guidance literature:: With 2,6-dimethylpyridine; In dichloromethane; at 0 - 20 ℃; for 2h;
DOI:10.1016/j.tetasy.2005.12.020

Reference yield:

: 14425-64-0
4-methoxyphenethyl bromide

: 882408-54-0
N-bis(trimethylsilyl)methyl-N-[2-(4-methoxyphenyl)ethyl]-α-methoxycarbonyl-α-diazoacetamide

Guidance literature:: Multi-step reaction with 2 steps

1: 54 percent / Na₂CO₃; NaI / dimethylformamide

2: 85 percent / 2,6-lutidine / CH₂Cl₂ / 2 h / 0 - 20 °C

With 2,6-dimethylpyridine; sodium carbonate; sodium iodide; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.tetasy.2005.12.020

Reference yield:

: 134340-00-4
bis(trimethylsilyl)methylamine

: 882408-54-0
N-bis(trimethylsilyl)methyl-N-[2-(4-methoxyphenyl)ethyl]-α-methoxycarbonyl-α-diazoacetamide

Guidance literature:: Multi-step reaction with 2 steps

1: 54 percent / Na₂CO₃; NaI / dimethylformamide

2: 85 percent / 2,6-lutidine / CH₂Cl₂ / 2 h / 0 - 20 °C

With 2,6-dimethylpyridine; sodium carbonate; sodium iodide; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.tetasy.2005.12.020