1-Hydroxy-4-(2-oxo-2-phenyl-1-chloroethylidene)-2,2,5,5-tetramethylimidazolidine

Base Information

Chemical Name:1-Hydroxy-4-(2-oxo-2-phenyl-1-chloroethylidene)-2,2,5,5-tetramethylimidazolidine
CAS No.:127720-71-2
Molecular Formula:C₁₅H₁₉ClN₂O₂
Molecular Weight:294.781
Hs Code.:

Synonyms:1-Hydroxy-4-(2-oxo-2-phenyl-1-chloroethylidene)-2,2,5,5-tetramethylimidazolidine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-Hydroxy-4-(2-oxo-2-phenyl-1-chloroethylidene)-2,2,5,5-tetramethylimidazolidine

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Technology Process of 1-Hydroxy-4-(2-oxo-2-phenyl-1-chloroethylidene)-2,2,5,5-tetramethylimidazolidine

There total 1 articles about 1-Hydroxy-4-(2-oxo-2-phenyl-1-chloroethylidene)-2,2,5,5-tetramethylimidazolidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 84359-72-8
4-(2-Oxo-2-phenyl-1-chloroethylidene)-2,2,5,5-tetramethylimidazolidine-1-oxyl

: 127720-71-2
1-Hydroxy-4-(2-oxo-2-phenyl-1-chloroethylidene)-2,2,5,5-tetramethylimidazolidine

Guidance literature:: With zinc;
DOI:10.1007/BF00960664

Reference yield: 83.0%

: 127720-71-2
1-Hydroxy-4-(2-oxo-2-phenyl-1-chloroethylidene)-2,2,5,5-tetramethylimidazolidine

: 127720-70-1
3-chloro-1-hydroxy-5,5-dimethyl-4-oxo-2-pentafluorophenylpyrroline

Guidance literature:: With hydrogenchloride; In methanol; at 20 ℃; for 10h;
DOI:10.1007/BF02499074

Reference yield:

: 127720-71-2
1-Hydroxy-4-(2-oxo-2-phenyl-1-chloroethylidene)-2,2,5,5-tetramethylimidazolidine

: 129994-12-3
4-[3-(5,5-dimethyl-1-oxido-4-oxo-2-phenyl-4,5-dihydro-3H-pyrrol-3-ylidene)-5,5-dimethyl-1-oxido-4-oxo-4,5-dihydro-3H-pyrrol-2-yl]benzoic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 83 percent / 10 percent HCl / methanol / 10 h / 20 °C

2: 50 percent / NaCN; 15-crown-5-ether / acetonitrile / 2 h / 20 °C

With hydrogenchloride; 15-crown-5; sodium cyanide; In methanol; acetonitrile; 1: Ring cleavage / 2: Dimerization;
DOI:10.1007/BF02499074