N^α-benzyloxycarbonyltryptophyl-N^G-nitroarginylalanine p-nitrobenzyl ester

Base Information

Chemical Name:N^α-benzyloxycarbonyltryptophyl-N^G-nitroarginylalanine p-nitrobenzyl ester
CAS No.:102249-06-9
Molecular Formula:C₃₅H₃₉N₉O₁₀
Molecular Weight:745.749
Hs Code.:

N<sup>α</sup>-benzyloxycarbonyltryptophyl-N<sup>G</sup>-nitroarginylalanine p-nitrobenzyl ester

Synonyms:N^α-benzyloxycarbonyltryptophyl-N^G-nitroarginylalanine p-nitrobenzyl ester

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Chemical Property of N^α-benzyloxycarbonyltryptophyl-N^G-nitroarginylalanine p-nitrobenzyl ester

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Technology Process of N^α-benzyloxycarbonyltryptophyl-N^G-nitroarginylalanine p-nitrobenzyl ester

There total 4 articles about N^α-benzyloxycarbonyltryptophyl-N^G-nitroarginylalanine p-nitrobenzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

: 102249-17-2
C₁₆H₂₃N₇O₇*BrH

: 16624-64-9
N-α-carbobenzoxy-L-tyrosine p-nitrophenyl ester

: 102249-06-9
N^α-benzyloxycarbonyltryptophyl-N^G-nitroarginylalanine p-nitrobenzyl ester

Guidance literature:: With triethylamine; In N,N-dimethyl-formamide; at 18 - 25 ℃; for 24h;

Reference yield:

: 46744-54-1
L-Ala-ONB

: 102249-06-9
N^α-benzyloxycarbonyltryptophyl-N^G-nitroarginylalanine p-nitrobenzyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 53 percent / Et₃N, dicyclohexylcarbodiimide / CHCl₃ / 12 h / 18 - 25 °C / DMF used as solvent as well

2: HBr / acetic acid / 1 h / 20 °C

3: 51 percent / Et₃N / dimethylformamide / 24 h / 18 - 25 °C

With hydrogen bromide; triethylamine; dicyclohexyl-carbodiimide; In chloroform; acetic acid; N,N-dimethyl-formamide;

Reference yield:

: 2304-98-5
N₅-[imino(nitroamino)methyl]-N₂-[(phenylmethoxy)carbonyl]-L-ornithine

: 102249-06-9
N^α-benzyloxycarbonyltryptophyl-N^G-nitroarginylalanine p-nitrobenzyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 53 percent / Et₃N, dicyclohexylcarbodiimide / CHCl₃ / 12 h / 18 - 25 °C / DMF used as solvent as well

2: HBr / acetic acid / 1 h / 20 °C

3: 51 percent / Et₃N / dimethylformamide / 24 h / 18 - 25 °C

With hydrogen bromide; triethylamine; dicyclohexyl-carbodiimide; In chloroform; acetic acid; N,N-dimethyl-formamide;