methyl 2-(3,5-dimethoxy-1-methyloxycarbonyl-4-oxo-2,5-cyclohexadienyl)ace

Base Information

Chemical Name:methyl 2-(3,5-dimethoxy-1-methyloxycarbonyl-4-oxo-2,5-cyclohexadienyl)ace
CAS No.:358742-96-8
Molecular Formula:C₁₃H₁₆O₇
Molecular Weight:284.266
Hs Code.:

Synonyms:methyl 2-(3,5-dimethoxy-1-methyloxycarbonyl-4-oxo-2,5-cyclohexadienyl)ace

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Chemical Property of methyl 2-(3,5-dimethoxy-1-methyloxycarbonyl-4-oxo-2,5-cyclohexadienyl)ace

Chemical Property:

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MSDS Files:: SDS file from LookChem

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Technology Process of methyl 2-(3,5-dimethoxy-1-methyloxycarbonyl-4-oxo-2,5-cyclohexadienyl)ace

There total 1 articles about methyl 2-(3,5-dimethoxy-1-methyloxycarbonyl-4-oxo-2,5-cyclohexadienyl)ace which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 44.0%

: 358742-91-3
methyl 2-(3,5-dimethoxy-1-methyloxycarbonyl-2,5-cyclohexadienyl)acetate

: 358742-96-8
methyl 2-(3,5-dimethoxy-1-methyloxycarbonyl-4-oxo-2,5-cyclohexadienyl)ace

Guidance literature:: With tert.-butylhydroperoxide; dipyridinium dichromate; Celite; triethylamine; In benzene; at 20 ℃; for 6h;
DOI:10.1081/SCC-100000539

Reference yield: 75.0%

: 358742-96-8
methyl 2-(3,5-dimethoxy-1-methyloxycarbonyl-4-oxo-2,5-cyclohexadienyl)ace

: 4385-56-2
2-(4-hydroxy-3,5-dimethoxyphenyl)acetic acid

Guidance literature:: With sodium hydroxide; In ethanol; water; at 20 ℃; for 6h;
DOI:10.1081/SCC-100000539

Reference yield:

: 358742-96-8
methyl 2-(3,5-dimethoxy-1-methyloxycarbonyl-4-oxo-2,5-cyclohexadienyl)ace

: 488855-69-2
N-[3-(3,4-dimethyl-phenyl)-propyl]-2-(4-hydroxy-3,5-dimethoxy-phenyl)-acetamide

Guidance literature:: Multi-step reaction with 2 steps

1: aq. NaOH / methanol / 4 h / 0 - 20 °C

2: 77 percent / HOBt; DCC / acetonitrile / 0 - 20 °C

With sodium hydroxide; benzotriazol-1-ol; dicyclohexyl-carbodiimide; In methanol; acetonitrile;
DOI:10.1016/S0960-894X(02)00479-1