methyl 2-phenyl-3-ethylhexanoate

Base Information

• Chemical Name: methyl 2-phenyl-3-ethylhexanoate
• CAS No.: 1115295-58-3
• Molecular Formula: C₁₅H₂₂O₂
• Molecular Weight: 234.338
• Mol file: 1115295-58-3.mol

Synonyms:methyl 2-phenyl-3-ethylhexanoate

Chemical Property of methyl 2-phenyl-3-ethylhexanoate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

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Technology Process of methyl 2-phenyl-3-ethylhexanoate

There total 2 articles about methyl 2-phenyl-3-ethylhexanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 20.0%

hexane (110-54-3) + Methyl phenyldiazoacetate (22979-35-7) → methyl 2-phenyl-3-methylheptanoate (1115295-56-1) + methyl 2-phenyl-3-ethylhexanoate (1115295-58-3)

Guidance literature:

With iron(II) perchlorate hydrate; N,N'-dimethyl-N,N'-bis(2-pyridylmethyl)ethane-1,2-diamine; sodium tetrakis[(3,5-di-trifluoromethyl)phenyl]borate; In chloroform; for 48h; chemoselective reaction; Schlenk technique; Reflux;

DOI:10.1055/s-0036-1588743

Reference yield:

hexane (110-54-3) + Methyl phenyldiazoacetate (22979-35-7) → methyl 2-phenyloctanoate (936830-17-0) + methyl 2-phenyl-3-methylheptanoate (1115295-56-1) + methyl 2-phenyl-3-ethylhexanoate (1115295-58-3)

Guidance literature:

With (5,10,15,20-tetrakis-4-tolylporphyrinato)(methyl)rhodium(III); In 1,2-dichloro-ethane; at 80 ℃; for 24h; regioselective reaction; Inert atmosphere;

DOI:10.1002/anie.200803157

upstream raw materials:

hexane

Methyl phenyldiazoacetate