N-(2,6-dichlorobenzoyl)-4-(2-methoxyphenyl)-L-phenylalanine methyl ester

Base Information

• Chemical Name: N-(2,6-dichlorobenzoyl)-4-(2-methoxyphenyl)-L-phenylalanine methyl ester
• CAS No.: 232275-30-8
• Molecular Formula: C₂₄H₂₁Cl₂NO₄
• Molecular Weight: 458.341

Synonyms:N-(2,6-dichlorobenzoyl)-4-(2-methoxyphenyl)-L-phenylalanine methyl ester

Chemical Property of N-(2,6-dichlorobenzoyl)-4-(2-methoxyphenyl)-L-phenylalanine methyl ester

Chemical Property:

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Technology Process of N-(2,6-dichlorobenzoyl)-4-(2-methoxyphenyl)-L-phenylalanine methyl ester

There total 1 articles about N-(2,6-dichlorobenzoyl)-4-(2-methoxyphenyl)-L-phenylalanine methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2,6-Dichlorobenzoyl chloride (4659-45-4) + (S)-2-Amino-3-(2'-methoxy-biphenyl-4-yl)-propionic acid methyl ester; compound with trifluoro-acetic acid → N-(2,6-dichlorobenzoyl)-4-(2-methoxyphenyl)-L-phenylalanine methyl ester (232275-30-8)

Guidance literature:

With N-ethyl-N,N-diisopropylamine; In dichloromethane; at 20 ℃; for 24h;

DOI:10.1016/S0968-0896(02)00021-4

Reference yield:

N-(2,6-dichlorobenzoyl)-4-(2-methoxyphenyl)-L-phenylalanine methyl ester (232275-30-8) → N-(2,6-dichlorobenzoyl)-4-(2-hydroxyphenyl)-L-phenylalanine methyl ester (232276-12-9)

Guidance literature:

With boron tribromide; sodium hydrogencarbonate; In dichloromethane; ethyl acetate;

Reference yield:

N-(2,6-dichlorobenzoyl)-4-(2-methoxyphenyl)-L-phenylalanine methyl ester (232275-30-8) → N-(2,6-dichlorobenzoyl)-4-(2-methoxyphenyl)-L-phenylalanine (232271-13-5)

Guidance literature:

With lithium hydroxide; In tetrahydrofuran; methanol; at 20 ℃; for 3h;

DOI:10.1016/S0968-0896(02)00021-4

upstream raw materials:

2,6-Dichlorobenzoyl chloride

Downstream raw materials:

N-(2,6-dichlorobenzoyl)-4-(2-methoxyphenyl)-L-phenylalanine

N-(2,6-dichlorobenzoyl)-4-(2-hydroxyphenyl)-L-phenylalanine methyl ester

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