1-(4-butoxy-3,5-dimethoxybenzoyl)-2-(N,N-diethylamino)carbonyloxymethyl-4-triphenylmethylpiperazine

Base Information

Chemical Name:1-(4-butoxy-3,5-dimethoxybenzoyl)-2-(N,N-diethylamino)carbonyloxymethyl-4-triphenylmethylpiperazine
CAS No.:916974-77-1
Molecular Formula:C₄₂H₅₁N₃O₆
Molecular Weight:693.883
Hs Code.:

Synonyms:1-(4-butoxy-3,5-dimethoxybenzoyl)-2-(N,N-diethylamino)carbonyloxymethyl-4-triphenylmethylpiperazine

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Chemical Property of 1-(4-butoxy-3,5-dimethoxybenzoyl)-2-(N,N-diethylamino)carbonyloxymethyl-4-triphenylmethylpiperazine

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Technology Process of 1-(4-butoxy-3,5-dimethoxybenzoyl)-2-(N,N-diethylamino)carbonyloxymethyl-4-triphenylmethylpiperazine

There total 4 articles about 1-(4-butoxy-3,5-dimethoxybenzoyl)-2-(N,N-diethylamino)carbonyloxymethyl-4-triphenylmethylpiperazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.3%

: 916974-76-0
2-(N,N-diethylamino)carbonyloxymethyl-1-(4-hydroxy-3,5-dimethoxybenzoyl)-4-triphenylmethylpiperazine

: 109-65-9
1-bromo-butane

: 916974-77-1
1-(4-butoxy-3,5-dimethoxybenzoyl)-2-(N,N-diethylamino)carbonyloxymethyl-4-triphenylmethylpiperazine

Guidance literature:: With potassium carbonate; In acetone; for 6h; Heating;
DOI:10.1016/j.bmc.2006.07.031

Reference yield:

: 76-83-5
trityl chloride

: 916974-77-1
1-(4-butoxy-3,5-dimethoxybenzoyl)-2-(N,N-diethylamino)carbonyloxymethyl-4-triphenylmethylpiperazine

Guidance literature:: Multi-step reaction with 3 steps

1: 99.7 percent / triethylamine / CH₂Cl₂ / 6 h / 0 °C

2: 52.4 percent / N,N'-dicyclohexylcarbodiimide; 1-hydroxybenzotriazole / CH₂Cl₂ / Heating

3: 82.3 percent / K₂CO₃ / acetone / 6 h / Heating

With potassium carbonate; benzotriazol-1-ol; triethylamine; dicyclohexyl-carbodiimide; In dichloromethane; acetone;
DOI:10.1016/j.bmc.2006.07.031

Reference yield:

: 253873-18-6
3-(N,N-diethylaminocarbonyloxymethyl)-1-(triphenylmethyl)piperazine

: 916974-77-1
1-(4-butoxy-3,5-dimethoxybenzoyl)-2-(N,N-diethylamino)carbonyloxymethyl-4-triphenylmethylpiperazine

Guidance literature:: Multi-step reaction with 2 steps

1: 52.4 percent / N,N'-dicyclohexylcarbodiimide; 1-hydroxybenzotriazole / CH₂Cl₂ / Heating

2: 82.3 percent / K₂CO₃ / acetone / 6 h / Heating

With potassium carbonate; benzotriazol-1-ol; dicyclohexyl-carbodiimide; In dichloromethane; acetone;
DOI:10.1016/j.bmc.2006.07.031