C₁₃H₁₈BNO₄

Base Information

• Chemical Name: C₁₃H₁₈BNO₄
• CAS No.: 1280078-59-2
• Molecular Formula: C₁₃H₁₈BNO₄
• Molecular Weight: 263.101
• Mol file: 1280078-59-2.mol

Synonyms:C₁₃H₁₈BNO₄

Chemical Property of C₁₃H₁₈BNO₄

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of C₁₃H₁₈BNO₄

There total 1 articles about C₁₃H₁₈BNO₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

p-bromobenzaldehyde 1,3-dioxolane (10602-01-4) + 2,2'-iminobis[ethanol] (111-42-2) → C13H18BNO4 (1280078-59-2)

Guidance literature:

p-bromobenzaldehyde 1,3-dioxolane; With n-butyllithium; In tetrahydrofuran; at -78 ℃; for 0.166667h; Inert atmosphere;

With Triisopropyl borate; In tetrahydrofuran; at -78 - 20 ℃; for 1h;

2,2'-iminobis[ethanol]; In diethyl ether; isopropyl alcohol;

DOI:10.1016/j.tetlet.2011.01.012

Reference yield: 93.0%

C13H18BNO4 (1280078-59-2) + 4-bromo-benzaldehyde (1122-91-4) → C16H14O3 (893737-04-7)

Guidance literature:

With bis-triphenylphosphine-palladium(II) chloride; potassium phosphate; copper(l) iodide; triphenylphosphine; In water; N,N-dimethyl-formamide; at 100 ℃; Inert atmosphere;

DOI:10.1016/j.tetlet.2011.01.012

upstream raw materials:

p-bromobenzaldehyde 1,3-dioxolane

2,2'-iminobis[ethanol]

Downstream raw materials:

C₁₆H₁₄O₃