{2-[2-(2-{2-[2-(2-hydroxy-ethylcarbamoyl)-ethoxy]-ethoxy}-ethoxy)-ethoxy]-ethyl}-carbamic acid benzyl ester

Base Information

Chemical Name:{2-[2-(2-{2-[2-(2-hydroxy-ethylcarbamoyl)-ethoxy]-ethoxy}-ethoxy)-ethoxy]-ethyl}-carbamic acid benzyl ester
CAS No.:709675-87-6
Molecular Formula:C₂₁H₃₄N₂O₈
Molecular Weight:442.51
Hs Code.:

Synonyms:{2-[2-(2-{2-[2-(2-hydroxy-ethylcarbamoyl)-ethoxy]-ethoxy}-ethoxy)-ethoxy]-ethyl}-carbamic acid benzyl ester

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Chemical Property of {2-[2-(2-{2-[2-(2-hydroxy-ethylcarbamoyl)-ethoxy]-ethoxy}-ethoxy)-ethoxy]-ethyl}-carbamic acid benzyl ester

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Technology Process of {2-[2-(2-{2-[2-(2-hydroxy-ethylcarbamoyl)-ethoxy]-ethoxy}-ethoxy)-ethoxy]-ethyl}-carbamic acid benzyl ester

There total 1 articles about {2-[2-(2-{2-[2-(2-hydroxy-ethylcarbamoyl)-ethoxy]-ethoxy}-ethoxy)-ethoxy]-ethyl}-carbamic acid benzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 756526-00-8,1334177-88-6
3-oxo-1-phenyl-2,7,10,13,16-pentaoxa-4-azanonadecan-19-oic acid

: 141-43-5
ethanolamine

: 709675-87-6
{2-[2-(2-{2-[2-(2-hydroxy-ethylcarbamoyl)-ethoxy]-ethoxy}-ethoxy)-ethoxy]-ethyl}-carbamic acid benzyl ester

Guidance literature:: 3-oxo-1-phenyl-2,7,10,13,16-pentaoxa-4-azanonadecan-19-oic acid; With benzotriazol-1-ol; diisopropyl-carbodiimide; In dichloromethane; N,N-dimethyl-formamide; for 0.25h;

ethanolamine; In dichloromethane; N,N-dimethyl-formamide; for 4h;
DOI:10.1021/ol060414i

Reference yield:

: 709675-87-6
{2-[2-(2-{2-[2-(2-hydroxy-ethylcarbamoyl)-ethoxy]-ethoxy}-ethoxy)-ethoxy]-ethyl}-carbamic acid benzyl ester

: N-{2-[2-(2-{2-[2-(2-{[3-(6-tert-butoxycarbonylamino-hexanoyloxy)-2-(tert-butyl-dimethyl-silanyloxy)-propoxy]-hydroxy-phosphoryloxy}-ethylcarbamoyl)-ethoxy]-ethoxy}-ethoxy)-ethoxy]-ethyl}-6-(6-hydroxy-3-oxo-3H-xanthen-9-yl)-isophthalamic acid

Guidance literature:: Multi-step reaction with 4 steps

1: 1H-tetrazole / CH₂Cl₂ / 1.5 h / 20 °C

2: 85.3 mg / m-chloroperbenzoic acid / CH₂Cl₂ / -40 - 20 °C

3: 94 percent / H₂ / Pd/C / H₂O; 2-methyl-propan-2-ol / 6 h / 2585.74 Torr

4: 11.3 mg / Et₃N / dimethylformamide

With 1H-tetrazole; hydrogen; triethylamine; 3-chloro-benzenecarboperoxoic acid; palladium on activated charcoal; In dichloromethane; water; N,N-dimethyl-formamide; tert-butyl alcohol;
DOI:10.1021/ol060414i

Reference yield:

: 709675-87-6
{2-[2-(2-{2-[2-(2-hydroxy-ethylcarbamoyl)-ethoxy]-ethoxy}-ethoxy)-ethoxy]-ethyl}-carbamic acid benzyl ester

: C₅₃H₇₆BF₂N₈O₁₄P

Guidance literature:: Multi-step reaction with 6 steps

1: 1H-tetrazole / CH₂Cl₂ / 1.5 h / 20 °C

2: 85.3 mg / m-chloroperbenzoic acid / CH₂Cl₂ / -40 - 20 °C

3: 94 percent / H₂ / Pd/C / H₂O; 2-methyl-propan-2-ol / 6 h / 2585.74 Torr

4: 60 percent / dimethylformamide

5: TFA / CH₂Cl₂ / 2 h

6: TEAB / dimethylformamide / 20 °C / pH 7.4

With 1H-tetrazole; tetraethylammonium bromide; hydrogen; 3-chloro-benzenecarboperoxoic acid; trifluoroacetic acid; palladium on activated charcoal; In dichloromethane; water; N,N-dimethyl-formamide; tert-butyl alcohol;
DOI:10.1021/ol060414i