C₃₃H₃₄ClNO₄

Base Information

Chemical Name:C₃₃H₃₄ClNO₄
CAS No.:1258935-42-0
Molecular Formula:C₃₃H₃₄ClNO₄
Molecular Weight:544.09
Hs Code.:

C<sub>33</sub>H<sub>34</sub>ClNO<sub>4</sub>

Synonyms:C₃₃H₃₄ClNO₄

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Chemical Property of C₃₃H₃₄ClNO₄

Chemical Property:

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Technology Process of C₃₃H₃₄ClNO₄

There total 16 articles about C₃₃H₃₄ClNO₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1196996-66-3
(3-(benzyloxy)-6-(((S)-7-(benzyloxy)-1,2,3,4-tetrahydro-6-methoxyisoquinolin-1-yl)-methyl)-2-methoxyphenyl)methanol

: 1258935-42-0
C₃₃H₃₄ClNO₄

Guidance literature:: With thionyl chloride; In dichloromethane; at 0 - 20 ℃;
DOI:10.1021/jo9020826

Reference yield:

: 1196996-65-2
3-(benzyloxy)-6-(((S)-7-(benzyloxy)-1,2,3,4-tetrahydro-6-methoxyisoquinolin-1-yl)methyl)-2-methoxybenzyl acetate

: 1258935-42-0
C₃₃H₃₄ClNO₄

Guidance literature:: Multi-step reaction with 2 steps

1: water; sodium hydroxide / ethanol / 3 h / 20 °C

2: thionyl chloride / dichloromethane / 1.5 h / 0 - 20 °C

With thionyl chloride; water; sodium hydroxide; In ethanol; dichloromethane;
DOI:10.1016/j.bmc.2012.12.016

Reference yield:

: 1196996-63-0
6-((4-(benzyloxy-3-methoxyphenethyl)carbamoyl)methyl)-3-(benzyloxy)-2-methoxybenzyl acetate

: 1258935-42-0
C₃₃H₃₄ClNO₄

Guidance literature:: Multi-step reaction with 4 steps

1: trichlorophosphate / acetonitrile / 1 h / Reflux; Inert atmosphere

2: (1S,2S)-(+)-N-tosyl-1,2-diphenylethane-1,2-diamine[η6-1-isopropyl-4-methylbenzene]-ruthenium(II); formic acid; triethylamine / N,N-dimethyl-formamide / 20 °C

3: water; sodium hydroxide / ethanol / 3 h / 20 °C

4: thionyl chloride / dichloromethane / 1.5 h / 0 - 20 °C

With (1S,2S)-(+)-N-tosyl-1,2-diphenylethane-1,2-diamine[η6-1-isopropyl-4-methylbenzene]-ruthenium(II); formic acid; thionyl chloride; water; triethylamine; sodium hydroxide; trichlorophosphate; In ethanol; dichloromethane; N,N-dimethyl-formamide; acetonitrile; 1: |Bischler-Napieralski Reaction;
DOI:10.1016/j.bmc.2012.12.016