Trifluoro-methanesulfonic acid (Z)-1-(2-oxo-oxazolidine-3-carbonyl)-2-phenyl-vinyl ester

Base Information

Chemical Name:Trifluoro-methanesulfonic acid (Z)-1-(2-oxo-oxazolidine-3-carbonyl)-2-phenyl-vinyl ester
CAS No.:914932-25-5
Molecular Formula:C₁₃H₁₀F₃NO₆S
Molecular Weight:365.287
Hs Code.:

Synonyms:Trifluoro-methanesulfonic acid (Z)-1-(2-oxo-oxazolidine-3-carbonyl)-2-phenyl-vinyl ester

Suppliers and Price of Trifluoro-methanesulfonic acid (Z)-1-(2-oxo-oxazolidine-3-carbonyl)-2-phenyl-vinyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of Trifluoro-methanesulfonic acid (Z)-1-(2-oxo-oxazolidine-3-carbonyl)-2-phenyl-vinyl ester

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of Trifluoro-methanesulfonic acid (Z)-1-(2-oxo-oxazolidine-3-carbonyl)-2-phenyl-vinyl ester

There total 3 articles about Trifluoro-methanesulfonic acid (Z)-1-(2-oxo-oxazolidine-3-carbonyl)-2-phenyl-vinyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: Trifluoro-methanesulfonic acid (Z)-1-chlorocarbonyl-2-phenyl-vinyl ester

: 497-25-6
dimethylenecyclourethane

: 914932-25-5
Trifluoro-methanesulfonic acid (Z)-1-(2-oxo-oxazolidine-3-carbonyl)-2-phenyl-vinyl ester

Guidance literature:: With n-butyllithium; In tetrahydrofuran; hexane; at -80 ℃; for 1h;
DOI:10.1016/j.tet.2006.07.085

Reference yield:

: 914932-23-3
(Z)-3-phenyl-2-(trifluoromethanesulfonyloxy)propenoic acid

: 914932-25-5
Trifluoro-methanesulfonic acid (Z)-1-(2-oxo-oxazolidine-3-carbonyl)-2-phenyl-vinyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: oxalyl chloride; DMF / CH₂Cl₂ / 1 h

2: 50 percent / n-butyllithium / tetrahydrofuran; hexane / 1 h / -80 °C

With n-butyllithium; oxalyl dichloride; N,N-dimethyl-formamide; In tetrahydrofuran; hexane; dichloromethane;
DOI:10.1016/j.tet.2006.07.085

Reference yield:

: 500130-99-4
methyl (Z)-3-phenyl-2-trifluoromethylsulfonyloxy propenoate

: 914932-25-5
Trifluoro-methanesulfonic acid (Z)-1-(2-oxo-oxazolidine-3-carbonyl)-2-phenyl-vinyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: LiOH / H₂O; tetrahydrofuran / 0.42 h / 0 - 20 °C

2: oxalyl chloride; DMF / CH₂Cl₂ / 1 h

3: 50 percent / n-butyllithium / tetrahydrofuran; hexane / 1 h / -80 °C

With lithium hydroxide; n-butyllithium; oxalyl dichloride; N,N-dimethyl-formamide; In tetrahydrofuran; hexane; dichloromethane; water;
DOI:10.1016/j.tet.2006.07.085