N-[N-{4-(4-methoxyphenyl)-3-chloro-2-oxo-azetidin-1-yl}acetamidyl]-5-nitroindazole

Base Information

Chemical Name:N-[N-{4-(4-methoxyphenyl)-3-chloro-2-oxo-azetidin-1-yl}acetamidyl]-5-nitroindazole
CAS No.:1277174-80-7
Molecular Formula:C₁₉H₁₆ClN₅O₅
Molecular Weight:429.82
Hs Code.:

Synonyms:N-[N-{4-(4-methoxyphenyl)-3-chloro-2-oxo-azetidin-1-yl}acetamidyl]-5-nitroindazole

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Chemical Property of N-[N-{4-(4-methoxyphenyl)-3-chloro-2-oxo-azetidin-1-yl}acetamidyl]-5-nitroindazole

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Technology Process of N-[N-{4-(4-methoxyphenyl)-3-chloro-2-oxo-azetidin-1-yl}acetamidyl]-5-nitroindazole

There total 4 articles about N-[N-{4-(4-methoxyphenyl)-3-chloro-2-oxo-azetidin-1-yl}acetamidyl]-5-nitroindazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 1245567-24-1
N-(N-(4-methoxybenzylideneamino)acetamidyl)-5-nitroindazole

: 79-04-9
chloroacetyl chloride

: 1277174-80-7
N-[N-{4-(4-methoxyphenyl)-3-chloro-2-oxo-azetidin-1-yl}acetamidyl]-5-nitroindazole

Guidance literature:: With triethylamine; for 0.0666667h; Microwave irradiation; Neat (no solvent);

Reference yield:

: 1245567-13-8
2-(5-nitroindazol-1-yl)acetohydrazide

: 1277174-80-7
N-[N-{4-(4-methoxyphenyl)-3-chloro-2-oxo-azetidin-1-yl}acetamidyl]-5-nitroindazole

Guidance literature:: Multi-step reaction with 2 steps

1: 0.03 h / Microwave irradiation; Neat (no solvent)

2: triethylamine / 0.07 h / Microwave irradiation; Neat (no solvent)

With triethylamine;

Reference yield:

: 126401-86-3
N-(ethyl ethanoate)-5-nitroindazole

: 1277174-80-7
N-[N-{4-(4-methoxyphenyl)-3-chloro-2-oxo-azetidin-1-yl}acetamidyl]-5-nitroindazole

Guidance literature:: Multi-step reaction with 3 steps

1: hydrazine hydrate / 0.06 h / Microwave irradiation; Neat (no solvent)

2: 0.03 h / Microwave irradiation; Neat (no solvent)

3: triethylamine / 0.07 h / Microwave irradiation; Neat (no solvent)

With hydrazine hydrate; triethylamine;