1-nitro-3-[(1Z,3E)-4-phenylbuta-1,3-dienyl]benzene

Base Information

Chemical Name:1-nitro-3-[(1Z,3E)-4-phenylbuta-1,3-dienyl]benzene
CAS No.:15866-63-4
Molecular Formula:C₁₆H₁₃NO₂
Molecular Weight:251.285
Hs Code.:
NSC Number:104466
DSSTox Substance ID:DTXSID10364347
Wikidata:Q82148261
Mol file:15866-63-4.mol

Synonyms:NSC104466;15866-63-4;DTXSID10364347;NSC-104466

Suppliers and Price of 1-nitro-3-[(1Z,3E)-4-phenylbuta-1,3-dienyl]benzene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 4 raw suppliers

Chemical Property of 1-nitro-3-[(1Z,3E)-4-phenylbuta-1,3-dienyl]benzene

Chemical Property:

Vapor Pressure:1.9E-07mmHg at 25°C
Boiling Point:437.6°C at 760 mmHg
Flash Point:209.3°C
Density:1.19g/cm³
XLogP3:5.2
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:3
Exact Mass:251.094628657
Heavy Atom Count:19
Complexity:337

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C(C=C1)C=CC=CC2=CC(=CC=C2)[N+](=O)[O-]
Isomeric SMILES:C1=CC=C(C=C1)/C=C/C=C\C2=CC(=CC=C2)[N+](=O)[O-]

Technology Process of 1-nitro-3-[(1Z,3E)-4-phenylbuta-1,3-dienyl]benzene

There total 3 articles about 1-nitro-3-[(1Z,3E)-4-phenylbuta-1,3-dienyl]benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1530-41-2
(3-nitrobenzyl)(triphenyl)phosphonium bromide

: 104-55-2
3-phenyl-propenal

: 15866-63-4
1-(m-Nitrophenyl)-4-phenyl-1,3-butadien

Guidance literature:: With lithium methanolate;
DOI:10.1139/v71-601

Reference yield:

: 3958-57-4
1-bromomethyl-3-nitrobenzene

: 15866-63-4
1-(m-Nitrophenyl)-4-phenyl-1,3-butadien

Guidance literature:: Multi-step reaction with 2 steps

1.1: acetonitrile / 21 - 23 °C / Inert atmosphere

2.1: n-butyllithium / hexane; tetrahydrofuran / 0.5 h / 0 °C

2.2: 0 - 20 °C / Cooling with ice

With n-butyllithium; In tetrahydrofuran; hexane; acetonitrile;
DOI:10.1002/adsc.201900631