Technology Process of C28H29N5O6
There total 13 articles about C28H29N5O6 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
tetrabutyl ammonium fluoride;
In
tetrahydrofuran;
at 20 ℃;
for 1h;
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: sodium t-butanolate / tetrahydrofuran / 1 h / Reflux
1.2: 2 h / -70 - 20 °C
2.1: sodium carbonate / (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / 1,2-dimethoxyethane; water / 70 °C / Inert atmosphere
3.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 1 h / 20 °C
4.1: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran / 20 °C
5.1: potassium carbonate / N,N-dimethyl-formamide / 4 h / 75 °C
6.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 1 h / 20 °C
With
di-isopropyl azodicarboxylate; tetrabutyl ammonium fluoride; sodium carbonate; potassium carbonate; triphenylphosphine; sodium t-butanolate;
(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride;
In
tetrahydrofuran; 1,2-dimethoxyethane; water; N,N-dimethyl-formamide;
2.1: Suzuki Coupling / 4.1: Mitsunobu reaction;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: sodium carbonate / (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / 1,2-dimethoxyethane; water / 70 °C / Inert atmosphere
2: tetrabutyl ammonium fluoride / tetrahydrofuran / 1 h / 20 °C
3: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran / 20 °C
4: potassium carbonate / N,N-dimethyl-formamide / 4 h / 75 °C
5: tetrabutyl ammonium fluoride / tetrahydrofuran / 1 h / 20 °C
With
di-isopropyl azodicarboxylate; tetrabutyl ammonium fluoride; sodium carbonate; potassium carbonate; triphenylphosphine;
(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride;
In
tetrahydrofuran; 1,2-dimethoxyethane; water; N,N-dimethyl-formamide;
1: Suzuki Coupling / 3: Mitsunobu reaction;