1,6-bis(m-vinylphenyl)hexane

Base Information

• Chemical Name: 1,6-bis(m-vinylphenyl)hexane
• CAS No.: 107270-51-9
• Molecular Formula: C₂₂H₂₆
• Molecular Weight: 290.448

Synonyms:1,6-bis(m-vinylphenyl)hexane

Chemical Property of 1,6-bis(m-vinylphenyl)hexane

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Technology Process of 1,6-bis(m-vinylphenyl)hexane

There total 6 articles about 1,6-bis(m-vinylphenyl)hexane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

1-(3-{6-[3-(1-Hydroxy-ethyl)-phenyl]-hexyl}-phenyl)-ethanol (107485-07-4) → 1,6-bis(m-vinylphenyl)hexane (107270-51-9)

Guidance literature:

With zinc(II) chloride; trichloroacetic acid; In dimethyl sulfoxide;

DOI:10.1246/bcsj.59.2035

Reference yield:

1 ,6-dibromohexane (629-03-8) → 1,6-bis(m-vinylphenyl)hexane (107270-51-9)

Guidance literature:

Multi-step reaction with 4 steps

1: Cu(I)Br / tetrahydrofuran; hexamethylphosphoric acid triamide / 4 h / Heating

2: 10 percent aq. HCl / dioxane / Ambient temperature

3: LiAlH₄ / diethyl ether

4: 50 percent / ZnCl₂, Cl₃CCOOH / dimethylsulfoxide

With hydrogenchloride; lithium aluminium tetrahydride; copper(I) bromide; zinc(II) chloride; trichloroacetic acid; In tetrahydrofuran; 1,4-dioxane; N,N,N,N,N,N-hexamethylphosphoric triamide; diethyl ether; dimethyl sulfoxide;

DOI:10.1246/bcsj.59.2035

Reference yield:

C10H11BrMgO2 (107484-93-5) → 1,6-bis(m-vinylphenyl)hexane (107270-51-9)

Guidance literature:

Multi-step reaction with 4 steps

1: Cu(I)Br / tetrahydrofuran; hexamethylphosphoric acid triamide / 4 h / Heating

2: 10 percent aq. HCl / dioxane / Ambient temperature

3: LiAlH₄ / diethyl ether

4: 50 percent / ZnCl₂, Cl₃CCOOH / dimethylsulfoxide

With hydrogenchloride; lithium aluminium tetrahydride; copper(I) bromide; zinc(II) chloride; trichloroacetic acid; In tetrahydrofuran; 1,4-dioxane; N,N,N,N,N,N-hexamethylphosphoric triamide; diethyl ether; dimethyl sulfoxide;

DOI:10.1246/bcsj.59.2035

upstream raw materials:

1,2-ethano<2.6>metacyclophane

1-(3-{6-[3-(1-Hydroxy-ethyl)-phenyl]-hexyl}-phenyl)-ethanol

1 ,6-dibromohexane

C₁₀H₁₁BrMgO₂

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