(E)-6-benzyloxycarbonylamino-4-tert-butoxycarbonylamino-hex-2-enoic acid tert-butyl ester

Base Information

Chemical Name:(E)-6-benzyloxycarbonylamino-4-tert-butoxycarbonylamino-hex-2-enoic acid tert-butyl ester
CAS No.:318514-25-9
Molecular Formula:C₂₃H₃₄N₂O₆
Molecular Weight:434.533
Hs Code.:

Synonyms:(E)-6-benzyloxycarbonylamino-4-tert-butoxycarbonylamino-hex-2-enoic acid tert-butyl ester

Suppliers and Price of (E)-6-benzyloxycarbonylamino-4-tert-butoxycarbonylamino-hex-2-enoic acid tert-butyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (E)-6-benzyloxycarbonylamino-4-tert-butoxycarbonylamino-hex-2-enoic acid tert-butyl ester

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (E)-6-benzyloxycarbonylamino-4-tert-butoxycarbonylamino-hex-2-enoic acid tert-butyl ester

There total 7 articles about (E)-6-benzyloxycarbonylamino-4-tert-butoxycarbonylamino-hex-2-enoic acid tert-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 318514-25-9
(E)-6-benzyloxycarbonylamino-4-tert-butoxycarbonylamino-hex-2-enoic acid tert-butyl ester

Guidance literature:: Multi-step reaction with 5 steps

1: 1M aq. NaOH / dioxane / 24 h / 20 °C

2: 4-methylmorpholine / tetrahydrofuran / 0.13 h

3: NaBH₄ / tetrahydrofuran; H₂O

4: DMSO; oxalyl chloride / CH₂Cl₂

5: CH₂Cl₂ / -45 - 20 °C

With 4-methyl-morpholine; sodium hydroxide; sodium tetrahydroborate; oxalyl dichloride; dimethyl sulfoxide; In tetrahydrofuran; 1,4-dioxane; dichloromethane; water;
DOI:10.1021/jm000078q

Reference yield:

: 95766-36-2
H-A₂bu(Z)-OH

: 318514-25-9
(E)-6-benzyloxycarbonylamino-4-tert-butoxycarbonylamino-hex-2-enoic acid tert-butyl ester

Guidance literature:: Multi-step reaction with 5 steps

1: 1M aq. NaOH / dioxane / 24 h / 20 °C

2: 4-methylmorpholine / tetrahydrofuran / 0.13 h

3: NaBH₄ / tetrahydrofuran; H₂O

4: DMSO; oxalyl chloride / CH₂Cl₂

5: CH₂Cl₂ / -45 - 20 °C

With 4-methyl-morpholine; sodium hydroxide; sodium tetrahydroborate; oxalyl dichloride; dimethyl sulfoxide; In tetrahydrofuran; 1,4-dioxane; dichloromethane; water;
DOI:10.1021/jm000078q

Reference yield:

: 47461-65-4
4-(((benzyloxy)carbonyl)amino)-2-((tert-butoxycarbonyl)amino)butanoic acid

: 318514-25-9
(E)-6-benzyloxycarbonylamino-4-tert-butoxycarbonylamino-hex-2-enoic acid tert-butyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 4-methylmorpholine / tetrahydrofuran / 0.13 h

2: NaBH₄ / tetrahydrofuran; H₂O

3: DMSO; oxalyl chloride / CH₂Cl₂

4: CH₂Cl₂ / -45 - 20 °C

With 4-methyl-morpholine; sodium tetrahydroborate; oxalyl dichloride; dimethyl sulfoxide; In tetrahydrofuran; dichloromethane; water;
DOI:10.1021/jm000078q