C₂₃H₃₂ClN₃O₃

Base Information

Chemical Name:C₂₃H₃₂ClN₃O₃
CAS No.:1359985-28-6
Molecular Formula:C₂₃H₃₂ClN₃O₃
Molecular Weight:433.978
Hs Code.:

C<sub>23</sub>H<sub>32</sub>ClN<sub>3</sub>O<sub>3</sub>

Synonyms:C₂₃H₃₂ClN₃O₃

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Chemical Property of C₂₃H₃₂ClN₃O₃

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Technology Process of C₂₃H₃₂ClN₃O₃

There total 17 articles about C₂₃H₃₂ClN₃O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: 1359985-26-4
2-[(1S,3S)-3-aminocyclohexyl]propan-2-ol

: 1359985-27-5
C₁₄H₁₅ClN₂O₃

: 1359985-28-6
C₂₃H₃₂ClN₃O₃

Guidance literature:: With O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; triethylamine; In N,N-dimethyl-formamide; at 20 ℃; for 16h;
DOI:10.1055/s-0031-1289884

Reference yield:

: C₁₀H₁₆O₄

: 1359985-28-6
C₂₃H₃₂ClN₃O₃

Guidance literature:: Multi-step reaction with 13 steps

1.1: diphenyl phosphoryl azide; triethylamine / toluene / 1 h / 70 °C

2.1: triethylamine / toluene / 5 h / 80 °C

3.1: lithium hydroxide monohydrate; water / tetrahydrofuran; methanol / 5 h / 20 °C

4.1: borane-THF / tetrahydrofuran / 4 h / -5 °C

5.1: Chiral Pak AD-H 250 column / ethanol; carbon dioxide / 40 °C / Resolution of racemate

6.1: palladium 10% on activated carbon; hydrogen / methanol / 16 h / 2585.81 Torr

7.1: acetic acid / toluene / 2 h / Reflux

8.1: tetrapropylammonium perruthennate; 4-methylmorpholine N-oxide / dichloromethane / 2 h / Molecular sieve

9.1: diethyl ether / 0.5 h / 0 °C

10.1: tetrapropylammonium perruthennate; 4-methylmorpholine N-oxide / dichloromethane / 2 h / Molecular sieve

11.1: diethyl ether / 0.5 h / 0 °C

12.1: hydroxylamine hydrochloride; triethylamine / water; isopropyl alcohol / 6 h / Reflux

12.2: 16 h / 0 °C

13.1: O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; triethylamine / N,N-dimethyl-formamide / 16 h / 20 °C

With tetrapropylammonium perruthennate; borane-THF; lithium hydroxide monohydrate; diphenyl phosphoryl azide; palladium 10% on activated carbon; hydroxylamine hydrochloride; water; hydrogen; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; acetic acid; 4-methylmorpholine N-oxide; triethylamine; In tetrahydrofuran; methanol; diethyl ether; ethanol; dichloromethane; carbon dioxide; water; N,N-dimethyl-formamide; isopropyl alcohol; toluene; 2.1: Curtius rearrangement / 9.1: Grignard reaction / 11.1: Grignard reaction;
DOI:10.1055/s-0031-1289884

Reference yield:

: 116724-13-1
trans rac-cyclohexyl 1,3-dicarboxylic acid

: 1359985-28-6
C₂₃H₃₂ClN₃O₃

Guidance literature:: Multi-step reaction with 14 steps

1.1: hydrogenchloride / water / 4 h / 80 °C

2.1: diphenyl phosphoryl azide; triethylamine / toluene / 1 h / 70 °C

3.1: triethylamine / toluene / 5 h / 80 °C

4.1: lithium hydroxide monohydrate; water / tetrahydrofuran; methanol / 5 h / 20 °C

5.1: borane-THF / tetrahydrofuran / 4 h / -5 °C

6.1: Chiral Pak AD-H 250 column / ethanol; carbon dioxide / 40 °C / Resolution of racemate

7.1: palladium 10% on activated carbon; hydrogen / methanol / 16 h / 2585.81 Torr

8.1: acetic acid / toluene / 2 h / Reflux

9.1: tetrapropylammonium perruthennate; 4-methylmorpholine N-oxide / dichloromethane / 2 h / Molecular sieve

10.1: diethyl ether / 0.5 h / 0 °C

11.1: tetrapropylammonium perruthennate; 4-methylmorpholine N-oxide / dichloromethane / 2 h / Molecular sieve

12.1: diethyl ether / 0.5 h / 0 °C

13.1: hydroxylamine hydrochloride; triethylamine / water; isopropyl alcohol / 6 h / Reflux

13.2: 16 h / 0 °C

14.1: O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; triethylamine / N,N-dimethyl-formamide / 16 h / 20 °C

With hydrogenchloride; tetrapropylammonium perruthennate; borane-THF; lithium hydroxide monohydrate; diphenyl phosphoryl azide; palladium 10% on activated carbon; hydroxylamine hydrochloride; water; hydrogen; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; acetic acid; 4-methylmorpholine N-oxide; triethylamine; In tetrahydrofuran; methanol; diethyl ether; ethanol; dichloromethane; carbon dioxide; water; N,N-dimethyl-formamide; isopropyl alcohol; toluene; 3.1: Curtius rearrangement / 10.1: Grignard reaction / 12.1: Grignard reaction;
DOI:10.1055/s-0031-1289884