C₂₉H₃₂N₈O₁₀

Base Information

Chemical Name:C₂₉H₃₂N₈O₁₀
CAS No.:1016557-33-7
Molecular Formula:C₂₉H₃₂N₈O₁₀
Molecular Weight:652.621
Hs Code.:

C<sub>29</sub>H<sub>32</sub>N<sub>8</sub>O<sub>10</sub>

Synonyms:C₂₉H₃₂N₈O₁₀

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₉H₃₂N₈O₁₀

Chemical Property:

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Technology Process of C₂₉H₃₂N₈O₁₀

There total 6 articles about C₂₉H₃₂N₈O₁₀ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 7776-34-3
L-proline hydrochloride

: 313644-33-6
C₁₉H₁₈N₆O₈

: 1016557-33-7
C₂₉H₃₂N₈O₁₀

Guidance literature:: C₁₉H₁₈N₆O₈; With oxalyl dichloride; N,N-dimethyl-formamide; In dichloromethane; at 0 - 20 ℃; for 2h;

L-proline hydrochloride; With triethylamine; In tetrahydrofuran; water; at 0 - 20 ℃; for 2h; Further stages.;
DOI:10.1016/j.tetlet.2008.01.004

Reference yield:

: 140658-44-2
1,1'-[(propane-1,3-diyl)dioxy]bis[(5-methoxy-2-nitro-1,4-phenylene)carbonyl]bis[(2S,4R)-methyl-4-hydroxypyrrolidine-2-carboxylate]

: 1016557-33-7
C₂₉H₃₂N₈O₁₀

Guidance literature:: Multi-step reaction with 5 steps

1.1: SnCl₄; HNO₃ / CH₂Cl₂ / 0.08 h / -25 °C

2.1: aq. NaNO₂; H₂SO₄ / 0 °C

2.2: NaN₃ / 0 °C

3.1: aq. NaOH

4.1: SOCl₂ / benzene / 3 h

5.1: Et₃N / tetrahydrofuran; H₂O / 1 h

With sodium hydroxide; thionyl chloride; sulfuric acid; nitric acid; tin(IV) chloride; triethylamine; sodium nitrite; In tetrahydrofuran; dichloromethane; water; benzene; 1.1: Reduction / 2.1: Diazotization / 2.2: Substitution / 3.1: Hydrolysis / 4.1: Chlorination / 5.1: Acylation;
DOI:10.1016/S0960-894X(00)00468-6

Reference yield:

: 909797-72-4
C₂₁H₂₆N₂O₈

: 1016557-33-7
C₂₉H₃₂N₈O₁₀

Guidance literature:: Multi-step reaction with 4 steps

1.1: aq. NaNO₂; H₂SO₄ / 0 °C

1.2: NaN₃ / 0 °C

2.1: aq. NaOH

3.1: SOCl₂ / benzene / 3 h

4.1: Et₃N / tetrahydrofuran; H₂O / 1 h

With sodium hydroxide; thionyl chloride; sulfuric acid; triethylamine; sodium nitrite; In tetrahydrofuran; water; benzene; 1.1: Diazotization / 1.2: Substitution / 2.1: Hydrolysis / 3.1: Chlorination / 4.1: Acylation;
DOI:10.1016/S0960-894X(00)00468-6