1-((Benzyloxycarbonyl)amino)-2-hydroxy-2-phenylethyl 4-methylphenyl ketone

Base Information

Chemical Name:1-((Benzyloxycarbonyl)amino)-2-hydroxy-2-phenylethyl 4-methylphenyl ketone
CAS No.:152528-98-8
Molecular Formula:C₂₄H₂₃NO₄
Molecular Weight:389.451
Hs Code.:

Synonyms:1-((Benzyloxycarbonyl)amino)-2-hydroxy-2-phenylethyl 4-methylphenyl ketone

Suppliers and Price of 1-((Benzyloxycarbonyl)amino)-2-hydroxy-2-phenylethyl 4-methylphenyl ketone

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 1-((Benzyloxycarbonyl)amino)-2-hydroxy-2-phenylethyl 4-methylphenyl ketone

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 1-((Benzyloxycarbonyl)amino)-2-hydroxy-2-phenylethyl 4-methylphenyl ketone

There total 1 articles about 1-((Benzyloxycarbonyl)amino)-2-hydroxy-2-phenylethyl 4-methylphenyl ketone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.9%

: 100-52-7
benzaldehyde

: 152528-95-5
2-oxo-2-p-tolyl-ethyl-carbamic acid benzyl ester

: 152528-98-8
1-((Benzyloxycarbonyl)amino)-2-hydroxy-2-phenylethyl 4-methylphenyl ketone

Guidance literature:: With sodium hexamethyldisilazane; In tetrahydrofuran; 1.) -50 deg C, 30 min, 2.) -50 to -40 deg C, 1 h;
DOI:10.1021/jo00075a032

Reference yield:

: 152528-98-8
1-((Benzyloxycarbonyl)amino)-2-hydroxy-2-phenylethyl 4-methylphenyl ketone

: 152529-00-5
1-(1-Hydroxybenzyl)-2-(4-methylphenyl)ethylenediamine

Guidance literature:: Multi-step reaction with 2 steps

1: NH₂OH*HCl, pyridine / ethanol / 7 h / Heating

2: H₂, conc. aq. HCl / 10percent Pd/C / 5 h / 2660 Torr / Ambient temperature

With pyridine; hydrogenchloride; hydroxylamine hydrochloride; hydrogen; palladium on activated charcoal; In ethanol;
DOI:10.1021/jo00075a032

Reference yield:

: 152528-98-8
1-((Benzyloxycarbonyl)amino)-2-hydroxy-2-phenylethyl 4-methylphenyl ketone

: 2-(4-Chlorophenyl)-4-(1-hydroxybenzyl)-5-(4-methylphenyl)imidazoline

Guidance literature:: Multi-step reaction with 3 steps

1: NH₂OH*HCl, pyridine / ethanol / 7 h / Heating

2: H₂, conc. aq. HCl / 10percent Pd/C / 5 h / 2660 Torr / Ambient temperature

3: Et₃N / 3 h / Heating

With pyridine; hydrogenchloride; hydroxylamine hydrochloride; hydrogen; triethylamine; palladium on activated charcoal; In ethanol;
DOI:10.1021/jo00075a032