N'-{2-chloro-5-[3-(3,5-dichlorophenyl)-4,4,4-trifluorobut-2-enoyl]phenyl}-4,4,4-trifluorobutanehydrazide

Base Information

Chemical Name:N'-{2-chloro-5-[3-(3,5-dichlorophenyl)-4,4,4-trifluorobut-2-enoyl]phenyl}-4,4,4-trifluorobutanehydrazide
CAS No.:1415107-34-4
Molecular Formula:C₂₀H₁₃Cl₃F₆N₂O₂
Molecular Weight:533.685
Hs Code.:

Synonyms:N'-{2-chloro-5-[3-(3,5-dichlorophenyl)-4,4,4-trifluorobut-2-enoyl]phenyl}-4,4,4-trifluorobutanehydrazide

Suppliers and Price of N'-{2-chloro-5-[3-(3,5-dichlorophenyl)-4,4,4-trifluorobut-2-enoyl]phenyl}-4,4,4-trifluorobutanehydrazide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of N'-{2-chloro-5-[3-(3,5-dichlorophenyl)-4,4,4-trifluorobut-2-enoyl]phenyl}-4,4,4-trifluorobutanehydrazide

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of N'-{2-chloro-5-[3-(3,5-dichlorophenyl)-4,4,4-trifluorobut-2-enoyl]phenyl}-4,4,4-trifluorobutanehydrazide

There total 5 articles about N'-{2-chloro-5-[3-(3,5-dichlorophenyl)-4,4,4-trifluorobut-2-enoyl]phenyl}-4,4,4-trifluorobutanehydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1415107-33-3
tert-butyl N-{2-chloro-5-[3-(3,5-dichlorophenyl)-4,4,4-trifluoro-3-hydroxybutanoyl]phenyl}-N'-(4,4,4-trifluorobutanoyl)carbazate

: 1415107-34-4
N'-{2-chloro-5-[3-(3,5-dichlorophenyl)-4,4,4-trifluorobut-2-enoyl]phenyl}-4,4,4-trifluorobutanehydrazide

Guidance literature:: tert-butyl N-{2-chloro-5-[3-(3,5-dichlorophenyl)-4,4,4-trifluoro-3-hydroxybutanoyl]phenyl}-N'-(4,4,4-trifluorobutanoyl)carbazate; With dmap; di-tert-butyl dicarbonate; triethylamine; In tetrahydrofuran; at 20 ℃; for 1.5h;

With trifluoroacetic acid; at 20 ℃; for 0.5h;

Reference yield:

: 1415107-32-2
tert-butyl N-(5-acetyl-2-chlorophenyl)-N'-(4,4,4-trifluorobutanoyl)carbazate

: 1415107-34-4
N'-{2-chloro-5-[3-(3,5-dichlorophenyl)-4,4,4-trifluorobut-2-enoyl]phenyl}-4,4,4-trifluorobutanehydrazide

Guidance literature:: Multi-step reaction with 2 steps

1.1: triethylamine / tetrahydrofuran / 4 h / 60 °C

2.1: triethylamine; di-tert-butyl dicarbonate; dmap / tetrahydrofuran / 1.5 h / 20 °C

2.2: 0.5 h / 20 °C

With dmap; di-tert-butyl dicarbonate; triethylamine; In tetrahydrofuran;

Reference yield:

: 1415107-30-0
tert-butyl N-(5-acetyl-2-chlorophenyl)carbamate

: 1415107-34-4
N'-{2-chloro-5-[3-(3,5-dichlorophenyl)-4,4,4-trifluorobut-2-enoyl]phenyl}-4,4,4-trifluorobutanehydrazide

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium hydroxide; ammonia; ammonium chloride; Aliquat 336; sodium hypochlorite / tetrahydrofuran; water / 12.3 h / 20 °C

2.1: triethylamine / tetrahydrofuran / 0.5 h / Cooling with ice

3.1: triethylamine / tetrahydrofuran / 4 h / 60 °C

4.1: triethylamine; di-tert-butyl dicarbonate; dmap / tetrahydrofuran / 1.5 h / 20 °C

4.2: 0.5 h / 20 °C

With dmap; sodium hypochlorite; di-tert-butyl dicarbonate; ammonia; Aliquat 336; ammonium chloride; triethylamine; sodium hydroxide; In tetrahydrofuran; water;