N′-{5-[5-(3,5-dichlorophenyl)-5-trifluoromethyl-4,5-dihydroisoxazol-3-yl]-2-chlorophenyl}-4,4,4-trifluorobutyrohydrazide

Base Information

Chemical Name:N′-{5-[5-(3,5-dichlorophenyl)-5-trifluoromethyl-4,5-dihydroisoxazol-3-yl]-2-chlorophenyl}-4,4,4-trifluorobutyrohydrazide
CAS No.:1237587-29-9
Molecular Formula:C₂₀H₁₄Cl₃F₆N₃O₂
Molecular Weight:548.699
Hs Code.:

Synonyms:N′-{5-[5-(3,5-dichlorophenyl)-5-trifluoromethyl-4,5-dihydroisoxazol-3-yl]-2-chlorophenyl}-4,4,4-trifluorobutyrohydrazide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N′-{5-[5-(3,5-dichlorophenyl)-5-trifluoromethyl-4,5-dihydroisoxazol-3-yl]-2-chlorophenyl}-4,4,4-trifluorobutyrohydrazide

Chemical Property:

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Technology Process of N′-{5-[5-(3,5-dichlorophenyl)-5-trifluoromethyl-4,5-dihydroisoxazol-3-yl]-2-chlorophenyl}-4,4,4-trifluorobutyrohydrazide

There total 12 articles about N′-{5-[5-(3,5-dichlorophenyl)-5-trifluoromethyl-4,5-dihydroisoxazol-3-yl]-2-chlorophenyl}-4,4,4-trifluorobutyrohydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 406-91-7
4,4,4-trifluorobutanoyl chloride

: 1237587-85-7
5-[5-(3,5-dichlorophenyl)-5-trifluoromethyl-4,5-dihydroisoxazol-3-yl]-2-chlorophenylhydrazine

: 1237587-29-9
N′-{5-[5-(3,5-dichlorophenyl)-5-trifluoromethyl-4,5-dihydroisoxazol-3-yl]-2-chlorophenyl}-4,4,4-trifluorobutyrohydrazide

Guidance literature:: With triethylamine; In tetrahydrofuran; at 0 - 20 ℃;

Reference yield:

: 1415107-34-4
N'-{2-chloro-5-[3-(3,5-dichlorophenyl)-4,4,4-trifluorobut-2-enoyl]phenyl}-4,4,4-trifluorobutanehydrazide

: 1237587-29-9
N′-{5-[5-(3,5-dichlorophenyl)-5-trifluoromethyl-4,5-dihydroisoxazol-3-yl]-2-chlorophenyl}-4,4,4-trifluorobutyrohydrazide

Guidance literature:: With hydroxylamine hydrochloride; tetrabutylammomium bromide; sodium hydroxide; In tert-butyl methyl ether; water; at 20 ℃; for 1h; Cooling with ice;

Reference yield:

: 864725-22-4
1,3-dichloro-5-(3,3,3-trifluoroprop-1-en-2-yl)benzene

: 1237587-29-9
N′-{5-[5-(3,5-dichlorophenyl)-5-trifluoromethyl-4,5-dihydroisoxazol-3-yl]-2-chlorophenyl}-4,4,4-trifluorobutyrohydrazide

Guidance literature:: Multi-step reaction with 4 steps

1.1: N-chloro-succinimide / N,N-dimethyl-formamide / 1 h / 60 °C

1.2: 6 h / 20 °C

2.1: water; acetic acid; iron / ethanol / 0.83 h / 75 °C

3.1: hydrogenchloride / 1,4-dioxane / 0.33 h / 20 °C

3.2: 0.25 h / 0 °C

4.1: triethylamine / tetrahydrofuran / 2 h / 0 - 20 °C

With hydrogenchloride; N-chloro-succinimide; water; iron; acetic acid; triethylamine; In tetrahydrofuran; 1,4-dioxane; ethanol; N,N-dimethyl-formamide;