4-cyano-3-(trimethylsilyl)phenylboronic acid

Base Information

Chemical Name:4-cyano-3-(trimethylsilyl)phenylboronic acid
CAS No.:1057732-41-8
Molecular Formula:C₁₀H₁₄BNO₂Si
Molecular Weight:219.123
Hs Code.:

Synonyms:4-cyano-3-(trimethylsilyl)phenylboronic acid

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-cyano-3-(trimethylsilyl)phenylboronic acid

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Technology Process of 4-cyano-3-(trimethylsilyl)phenylboronic acid

There total 2 articles about 4-cyano-3-(trimethylsilyl)phenylboronic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 1057732-31-6
4-bromo-2-(trimethylsilyl)benzonitrile

: 1057732-41-8
4-cyano-3-(trimethylsilyl)phenylboronic acid

Guidance literature:: 4-bromo-2-(trimethylsilyl)benzonitrile; With n-butyllithium; In tetrahydrofuran; at -70 ℃; for 0.25h;

With Trimethyl borate; In tetrahydrofuran; at -70 ℃;

With sulfuric acid; In tetrahydrofuran; at 20 ℃; Further stages.;
DOI:10.1021/jo8013808

Reference yield:

: 121-43-7,63156-11-6
Trimethyl borate

: 7732-18-5
water

: 1057732-41-8
4-cyano-3-(trimethylsilyl)phenylboronic acid

Guidance literature:: With H₃O⁽¹⁺⁾; In not given; (Ar); treating lihium deriv. with borate deriv., treatment with aq. acidsoln.; S. Lulinsky, K. Zajac, J. Org. Chem., 73 (2008) 7785-7788; S. Lu linsky, I. Madura, J. Serwatowski, H. Szatylowicz., J. Zachara, New. J. Chem., 31 (2007) 144-154;
DOI:10.1016/j.jorganchem.2010.08.016