C₂₄H₂₄N₂O₃S

Base Information

Chemical Name:C₂₄H₂₄N₂O₃S
CAS No.:1440510-50-8
Molecular Formula:C₂₄H₂₄N₂O₃S
Molecular Weight:420.532
Hs Code.:

C<sub>24</sub>H<sub>24</sub>N<sub>2</sub>O<sub>3</sub>S

Synonyms:C₂₄H₂₄N₂O₃S

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Chemical Property of C₂₄H₂₄N₂O₃S

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Technology Process of C₂₄H₂₄N₂O₃S

There total 4 articles about C₂₄H₂₄N₂O₃S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 542-69-8
1-iodo-butane

: 1065005-93-7
C₂₀H₁₆N₂O₃S

: 1440510-50-8
C₂₄H₂₄N₂O₃S

Guidance literature:: C₂₀H₁₆N₂O₃S; With sodium hydride; In tetrahydrofuran; N,N-dimethyl-formamide; at 60 ℃; for 0.5h; Inert atmosphere;

1-iodo-butane; In tetrahydrofuran; N,N-dimethyl-formamide; at 85 ℃; for 48h; Inert atmosphere;
DOI:10.1021/ol400849a

Reference yield:

: 90-02-8
salicylaldehyde

: 1440510-50-8
C₂₄H₂₄N₂O₃S

Guidance literature:: Multi-step reaction with 3 steps

1.1: trifluoroacetic acid / ethanol / Reflux; Inert atmosphere

2.1: triethylamine / dichloromethane / 1 h / 0 - 20 °C / Inert atmosphere

3.1: sodium hydride / N,N-dimethyl-formamide; tetrahydrofuran / 0.5 h / 60 °C / Inert atmosphere

3.2: 48 h / 85 °C / Inert atmosphere

With sodium hydride; triethylamine; trifluoroacetic acid; In tetrahydrofuran; ethanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/ol400849a

Reference yield:

: 2963-66-8
2-(2'-Hydroxyphenyl)benzimidazole

: 1440510-50-8
C₂₄H₂₄N₂O₃S

Guidance literature:: Multi-step reaction with 2 steps

1.1: triethylamine / dichloromethane / 1 h / 0 - 20 °C / Inert atmosphere

2.1: sodium hydride / N,N-dimethyl-formamide; tetrahydrofuran / 0.5 h / 60 °C / Inert atmosphere

2.2: 48 h / 85 °C / Inert atmosphere

With sodium hydride; triethylamine; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/ol400849a