(1R,2S,4S)-(+)-1-dicyclohexylsulfamoylmethyl-7,7-dimethylbicyclo<2.2.1>hept-2-yl hexadecanoate

Base Information

Chemical Name:(1R,2S,4S)-(+)-1-dicyclohexylsulfamoylmethyl-7,7-dimethylbicyclo<2.2.1>hept-2-yl hexadecanoate
CAS No.:172477-07-5
Molecular Formula:C₃₈H₆₉NO₄S
Molecular Weight:636.036
Hs Code.:

Synonyms:(1R,2S,4S)-(+)-1-dicyclohexylsulfamoylmethyl-7,7-dimethylbicyclo<2.2.1>hept-2-yl hexadecanoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (1R,2S,4S)-(+)-1-dicyclohexylsulfamoylmethyl-7,7-dimethylbicyclo<2.2.1>hept-2-yl hexadecanoate

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Technology Process of (1R,2S,4S)-(+)-1-dicyclohexylsulfamoylmethyl-7,7-dimethylbicyclo<2.2.1>hept-2-yl hexadecanoate

There total 1 articles about (1R,2S,4S)-(+)-1-dicyclohexylsulfamoylmethyl-7,7-dimethylbicyclo<2.2.1>hept-2-yl hexadecanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 99295-72-4
(+)-(1R,2S,4S)-N,N-dicyclohexyl-7,7-dimethyl-2-hydroxybicyclo[2.2.1]heptane-1-methanesulfonamide

: 112-67-4
n-hexadecanoyl chloride

: 172477-07-5
(1R,2S,4S)-(+)-1-dicyclohexylsulfamoylmethyl-7,7-dimethylbicyclo<2.2.1>hept-2-yl hexadecanoate

Guidance literature:: With silver cyanide; In toluene; for 6h; Heating;
DOI:10.1016/0957-4166(95)00305-9

Reference yield:

: 172477-07-5
(1R,2S,4S)-(+)-1-dicyclohexylsulfamoylmethyl-7,7-dimethylbicyclo<2.2.1>hept-2-yl hexadecanoate

: (1'R,2'S,4'S)-(+)-1'-dicyclohexylsulfamoylmethyl-7',7'-dimethylbicyclo<2.2.1>hept-2'-yl 2-bromohexadecanoate

Guidance literature:: With N-Bromosuccinimide; chloro-trimethyl-silane; lithium diisopropyl amide; Yield given. Multistep reaction;
DOI:10.1016/0957-4166(95)00305-9