7-methylsulfanyl-8,9,10-triazabicyclo[4.4.0]deca-1,3,5,7,9-pentaene

Base Information

• Chemical Name: 7-methylsulfanyl-8,9,10-triazabicyclo[4.4.0]deca-1,3,5,7,9-pentaene
• CAS No.: 22305-56-2
• Molecular Formula: C₈H₇N₃S
• Molecular Weight: 177.23
• Hs Code.: 2933699090
• Mol file: 22305-56-2.mol

Synonyms:4-(Methylthio)-1,2,3-benzotriazine;NSC 17809

Chemical Property of 7-methylsulfanyl-8,9,10-triazabicyclo[4.4.0]deca-1,3,5,7,9-pentaene

Chemical Property:

• Vapor Pressure: 4.8E-05mmHg at 25°C
• Boiling Point: 359.8°C at 760 mmHg
• Flash Point: 171.4°C
• PSA: 63.97000
• Density: 1.32g/cm³
• LogP: 1.74670

Purity/Quality:

99%min ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 7-methylsulfanyl-8,9,10-triazabicyclo[4.4.0]deca-1,3,5,7,9-pentaene

There total 2 articles about 7-methylsulfanyl-8,9,10-triazabicyclo[4.4.0]deca-1,3,5,7,9-pentaene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

methyl iodide (74-88-4) → 4-methylthio-1,2,3-benzotriazine (22305-56-2)

Guidance literature:

With sodium methylate; at 120 ℃;

Reference yield:

→ 4-methylthio-1,2,3-benzotriazine (22305-56-2)

Guidance literature:

1,2,3-Benzotriazin-4(3H)-thion (1), CH3I, NaOCH3;

Reference yield:

4-methylthio-1,2,3-benzotriazine (22305-56-2) → 4-Hydrazino-1,2,3-benzotriazin (55270-92-3)

Guidance literature:

With ethanol; hydrazine;

DOI:10.1021/jo01084a641

upstream raw materials:

methyl iodide

Downstream raw materials:

4-aminobenzo-1,2,3-triazine

4-Hydrazino-1,2,3-benzotriazin