Cbz-L-Orn{4-(2,3,4,6-tetra-O-benzyl-β-D-glucosyl)[1,2,3]triazol-1-yl}-OMe

Base Information

Chemical Name:Cbz-L-Orn{4-(2,3,4,6-tetra-O-benzyl-β-D-glucosyl)[1,2,3]triazol-1-yl}-OMe
CAS No.:917599-64-5
Molecular Formula:C₅₀H₅₄N₄O₉
Molecular Weight:855
Hs Code.:

Synonyms:Cbz-L-Orn{4-(2,3,4,6-tetra-O-benzyl-β-D-glucosyl)[1,2,3]triazol-1-yl}-OMe

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Chemical Property of Cbz-L-Orn{4-(2,3,4,6-tetra-O-benzyl-β-D-glucosyl)[1,2,3]triazol-1-yl}-OMe

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Technology Process of Cbz-L-Orn{4-(2,3,4,6-tetra-O-benzyl-β-D-glucosyl)[1,2,3]triazol-1-yl}-OMe

There total 3 articles about Cbz-L-Orn{4-(2,3,4,6-tetra-O-benzyl-β-D-glucosyl)[1,2,3]triazol-1-yl}-OMe which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 917599-62-3
Cbz-L-Orn(N₃)-OMe

: 168253-07-4
(2R,3R,4R,5S,6S)-3,4,5-Tris-benzyloxy-2-benzyloxymethyl-6-ethynyl-tetrahydro-pyran

: 917599-64-5
Cbz-L-Orn{4-(2,3,4,6-tetra-O-benzyl-β-D-glucosyl)[1,2,3]triazol-1-yl}-OMe

Guidance literature:: With copper diacetate; sodium L-ascorbate; In water; tert-butyl alcohol; at 20 ℃;
DOI:10.1055/s-2006-942509

Reference yield:

: 2640-58-6
Nα-benzyloxycarbonyl-L-ornithine

: 917599-64-5
Cbz-L-Orn{4-(2,3,4,6-tetra-O-benzyl-β-D-glucosyl)[1,2,3]triazol-1-yl}-OMe

Guidance literature:: Multi-step reaction with 3 steps

1: K₂CO₃; CuSO₄; TfN₃ / CH₂Cl₂; methanol; H₂O / 20 °C

2: 15.6 g / SOCl₂ / 4 h / Heating

3: 87 percent / Cu(OAc)2; sodium ascorbate / 2-methyl-propan-2-ol; H₂O / 20 °C

With thionyl chloride; copper diacetate; triflic azide; potassium carbonate; copper(II) sulfate; sodium L-ascorbate; In methanol; dichloromethane; water; tert-butyl alcohol; 3: Huisgen condensation;
DOI:10.1055/s-2006-942509

Reference yield:

: 1001646-61-2
5-azido-2-(((benzyloxy)carbonyl)amino)pentanoic acid

: 917599-64-5
Cbz-L-Orn{4-(2,3,4,6-tetra-O-benzyl-β-D-glucosyl)[1,2,3]triazol-1-yl}-OMe

Guidance literature:: Multi-step reaction with 2 steps

1: 15.6 g / SOCl₂ / 4 h / Heating

2: 87 percent / Cu(OAc)2; sodium ascorbate / 2-methyl-propan-2-ol; H₂O / 20 °C

With thionyl chloride; copper diacetate; sodium L-ascorbate; In water; tert-butyl alcohol; 2: Huisgen condensation;
DOI:10.1055/s-2006-942509