3-(2-isothiocyanatophenyl)-1-methyl-2-phenyl-5-(phenylthio)imidazolium-4-thiolate

Base Information

Chemical Name:3-(2-isothiocyanatophenyl)-1-methyl-2-phenyl-5-(phenylthio)imidazolium-4-thiolate
CAS No.:406480-96-4
Molecular Formula:C₂₃H₁₇N₃S₃
Molecular Weight:431.606
Hs Code.:

Synonyms:3-(2-isothiocyanatophenyl)-1-methyl-2-phenyl-5-(phenylthio)imidazolium-4-thiolate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-(2-isothiocyanatophenyl)-1-methyl-2-phenyl-5-(phenylthio)imidazolium-4-thiolate

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Technology Process of 3-(2-isothiocyanatophenyl)-1-methyl-2-phenyl-5-(phenylthio)imidazolium-4-thiolate

There total 1 articles about 3-(2-isothiocyanatophenyl)-1-methyl-2-phenyl-5-(phenylthio)imidazolium-4-thiolate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 71105-17-4
phenylene-1,2-diisothiocyanate

: 5-(tert-Butylamino)-3-methyl-4-phenyl-2-(phenylthio)thiazolium chloride

: 34858-80-5
13H-<1,3,5>thiodiazino<3,2-a,5,6-a'>bisbenzamidazole-13-thione

: 406480-96-4
3-(2-isothiocyanatophenyl)-1-methyl-2-phenyl-5-(phenylthio)imidazolium-4-thiolate

: 406480-97-5
1,2-bis[1-methyl-2-phenyl-5-(phenylthio)-4-thiolate-imidazolium-3-yl]phenyl

Guidance literature:: With triethylamine; In tetrahydrofuran; at 20 ℃; for 2h;
DOI:10.1002/hc.1093

Reference yield:

: 5-(tert-Butylamino)-3-methyl-4-phenyl-2-(phenylthio)thiazolium chloride

: 406480-96-4
3-(2-isothiocyanatophenyl)-1-methyl-2-phenyl-5-(phenylthio)imidazolium-4-thiolate

: 406480-97-5
1,2-bis[1-methyl-2-phenyl-5-(phenylthio)-4-thiolate-imidazolium-3-yl]phenyl

: C₄₃H₃₉N₅S₅

Guidance literature:: With triethylamine; In tetrahydrofuran; at 20 ℃; for 12h;
DOI:10.1002/hc.1093

Reference yield:

: 406480-96-4
3-(2-isothiocyanatophenyl)-1-methyl-2-phenyl-5-(phenylthio)imidazolium-4-thiolate

: 1,2-bis[1-methyl-4-(methylthio)-2-phenyl-5-(phenylthio)-4-thiolate-imidazolium-3-yl]phenyl diiodide

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / tetrahydrofuran / 12 h / 20 °C

2: CH₂Cl₂ / 0.17 h

With triethylamine; In tetrahydrofuran; dichloromethane;
DOI:10.1002/hc.1093