4,5-di-O-acetyl-2,6-benzyloxycarbonylimino-2,3,6-trideoxy-aldehydo-D-erythro-hex-2-enose

Base Information

Chemical Name:4,5-di-O-acetyl-2,6-benzyloxycarbonylimino-2,3,6-trideoxy-aldehydo-D-erythro-hex-2-enose
CAS No.:115710-38-8
Molecular Formula:C₁₈H₁₉NO₇
Molecular Weight:361.351
Hs Code.:

Synonyms:4,5-di-O-acetyl-2,6-benzyloxycarbonylimino-2,3,6-trideoxy-aldehydo-D-erythro-hex-2-enose

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Chemical Property of 4,5-di-O-acetyl-2,6-benzyloxycarbonylimino-2,3,6-trideoxy-aldehydo-D-erythro-hex-2-enose

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Technology Process of 4,5-di-O-acetyl-2,6-benzyloxycarbonylimino-2,3,6-trideoxy-aldehydo-D-erythro-hex-2-enose

There total 12 articles about 4,5-di-O-acetyl-2,6-benzyloxycarbonylimino-2,3,6-trideoxy-aldehydo-D-erythro-hex-2-enose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 17460-37-6
methyl 2-azido-4,6-O-benzylidene-2-deoxy-α-D-altropyranoside

: 115710-38-8
4,5-di-O-acetyl-2,6-benzyloxycarbonylimino-2,3,6-trideoxy-aldehydo-D-erythro-hex-2-enose

Guidance literature:: Multi-step reaction with 8 steps

1: 76 percent / 20percent acetic acid / H₂O / 1 h / 80 °C

2: 63 percent / pyridine

3: 91 percent / H₂ / 10percent Pd/C / ethanol / 2327.2 Torr

4: 4.7 g / sodium acetate / ethanol / Heating

5: sodium bicarbonate / ethanol; H₂O / 2 h

6: 77 percent / hydrochloric acid / CHCl₃ / 9 h

7: pyridine

8: mercuric chloride, cadmium carbonate / acetone; H₂O / 0.5 h / 80 °C

With hydrogenchloride; cadmium(II) carbonate; hydrogen; sodium acetate; sodium hydrogencarbonate; acetic acid; mercury dichloride; palladium on activated charcoal; In pyridine; ethanol; chloroform; water; acetone;
DOI:10.1016/S0040-4020(01)89805-7

Reference yield:

: 115684-45-2
3,4,5-tri-O-acetyl-2,6-benzyloxycarbonylimino-2,6-dideoxy-D-altrose diethyl dithioacetal

: 115710-38-8
4,5-di-O-acetyl-2,6-benzyloxycarbonylimino-2,3,6-trideoxy-aldehydo-D-erythro-hex-2-enose

Guidance literature:: With cadmium(II) carbonate; mercury dichloride; In water; acetone;
DOI:10.1016/S0040-4039(00)96576-6

Reference yield:

: 3075-59-0
methyl-2-azido-2-deoxy-α-D-altropyranoside

: 115710-38-8
4,5-di-O-acetyl-2,6-benzyloxycarbonylimino-2,3,6-trideoxy-aldehydo-D-erythro-hex-2-enose

Guidance literature:: Multi-step reaction with 7 steps

1: 63 percent / pyridine

2: 91 percent / H₂ / 10percent Pd/C / ethanol / 2327.2 Torr

3: 4.7 g / sodium acetate / ethanol / Heating

4: sodium bicarbonate / ethanol; H₂O / 2 h

5: 77 percent / hydrochloric acid / CHCl₃ / 9 h

6: pyridine

7: mercuric chloride, cadmium carbonate / acetone; H₂O / 0.5 h / 80 °C

With hydrogenchloride; cadmium(II) carbonate; hydrogen; sodium acetate; sodium hydrogencarbonate; mercury dichloride; palladium on activated charcoal; In pyridine; ethanol; chloroform; water; acetone;
DOI:10.1016/S0040-4020(01)89805-7