methyl <5-acetamido-4,7,8,9-tetra-O-acetyl-2-(phenoxycarbonyloxy)-3,5-dideoxy-β-D-glycero-D-galacto-2-nonulopyranosyl>onate

Base Information

Chemical Name:methyl <5-acetamido-4,7,8,9-tetra-O-acetyl-2-(phenoxycarbonyloxy)-3,5-dideoxy-β-D-glycero-D-galacto-2-nonulopyranosyl>onate
CAS No.:170298-66-5
Molecular Formula:C₂₇H₃₃NO₁₅
Molecular Weight:611.557
Hs Code.:

Synonyms:methyl <5-acetamido-4,7,8,9-tetra-O-acetyl-2-(phenoxycarbonyloxy)-3,5-dideoxy-β-D-glycero-D-galacto-2-nonulopyranosyl>onate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl <5-acetamido-4,7,8,9-tetra-O-acetyl-2-(phenoxycarbonyloxy)-3,5-dideoxy-β-D-glycero-D-galacto-2-nonulopyranosyl>onate

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Technology Process of methyl <5-acetamido-4,7,8,9-tetra-O-acetyl-2-(phenoxycarbonyloxy)-3,5-dideoxy-β-D-glycero-D-galacto-2-nonulopyranosyl>onate

There total 1 articles about methyl <5-acetamido-4,7,8,9-tetra-O-acetyl-2-(phenoxycarbonyloxy)-3,5-dideoxy-β-D-glycero-D-galacto-2-nonulopyranosyl>onate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 20298-34-4,84380-10-9
methyl (5-acetamido-4,7,8,9-tetra-O-acetyl-3,5-dideoxy-β-D-glycero-D-galacto-2-nonulopyranosyl)onate

: 1885-14-9
phenyl chloroformate

: 170298-66-5
methyl <5-acetamido-4,7,8,9-tetra-O-acetyl-2-(phenoxycarbonyloxy)-3,5-dideoxy-β-D-glycero-D-galacto-2-nonulopyranosyl>onate

Guidance literature:: With pyridine; In dichloromethane; at 0 ℃; for 5h;
DOI:10.1246/cl.1995.455

Reference yield: 22.0%

: 170298-66-5
methyl <5-acetamido-4,7,8,9-tetra-O-acetyl-2-(phenoxycarbonyloxy)-3,5-dideoxy-β-D-glycero-D-galacto-2-nonulopyranosyl>onate

: 73960-72-2
methyl-2,3-didehydro-4,7,8,9-tetra-O-acetyl-N-acetylneuraminate

: (2S,4S,5R,6R)-4-Acetoxy-5-acetylamino-2-cyclohexylmethoxy-6-((1S,2R)-1,2,3-triacetoxy-propyl)-tetrahydro-pyran-2-carboxylic acid methyl ester

: (2R,4S,5R,6R)-4-Acetoxy-5-acetylamino-2-cyclohexylmethoxy-6-((1S,2R)-1,2,3-triacetoxy-propyl)-tetrahydro-pyran-2-carboxylic acid methyl ester

Guidance literature:: With tetrachlorosilane; silver perchlorate; cyclohexylmethyl trimethylsilyl ether; In various solvent(s); at 0 ℃; for 2h; Yields of byproduct given;
DOI:10.1246/cl.1995.455

Reference yield: 22.0%

: 88773-80-2
cyclohexylmethyl trimethylsilyl ether

: 170298-66-5
methyl <5-acetamido-4,7,8,9-tetra-O-acetyl-2-(phenoxycarbonyloxy)-3,5-dideoxy-β-D-glycero-D-galacto-2-nonulopyranosyl>onate

: 73960-72-2
methyl-2,3-didehydro-4,7,8,9-tetra-O-acetyl-N-acetylneuraminate

: (2S,4S,5R,6R)-4-Acetoxy-5-acetylamino-2-cyclohexylmethoxy-6-((1S,2R)-1,2,3-triacetoxy-propyl)-tetrahydro-pyran-2-carboxylic acid methyl ester

: (2R,4S,5R,6R)-4-Acetoxy-5-acetylamino-2-cyclohexylmethoxy-6-((1S,2R)-1,2,3-triacetoxy-propyl)-tetrahydro-pyran-2-carboxylic acid methyl ester

Guidance literature:: With tetrachlorosilane; silver perchlorate; In various solvent(s); at 0 ℃; for 2h; Yield given. Yields of byproduct given;
DOI:10.1246/cl.1995.455