3,4,5-tri-O-benzyl-7-deoxy-7-fluoro-D-glycero-α-D-lyxo-hept-2-ulopyranose

Base Information

Chemical Name:3,4,5-tri-O-benzyl-7-deoxy-7-fluoro-D-glycero-α-D-lyxo-hept-2-ulopyranose
CAS No.:1357098-65-7
Molecular Formula:C₂₈H₃₁FO₆
Molecular Weight:482.549
Hs Code.:

Synonyms:3,4,5-tri-O-benzyl-7-deoxy-7-fluoro-D-glycero-α-D-lyxo-hept-2-ulopyranose

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Chemical Property of 3,4,5-tri-O-benzyl-7-deoxy-7-fluoro-D-glycero-α-D-lyxo-hept-2-ulopyranose

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Technology Process of 3,4,5-tri-O-benzyl-7-deoxy-7-fluoro-D-glycero-α-D-lyxo-hept-2-ulopyranose

There total 10 articles about 3,4,5-tri-O-benzyl-7-deoxy-7-fluoro-D-glycero-α-D-lyxo-hept-2-ulopyranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 1357098-64-6
3,4,5-tri-O-benzyl-2,6-anhydro-1,7-dideoxy-7-fluoro-D-mannohept-1-enitol

: 1357098-65-7
3,4,5-tri-O-benzyl-7-deoxy-7-fluoro-D-glycero-α-D-lyxo-hept-2-ulopyranose

Guidance literature:: With water; potassium carbonate; potassium hexacyanoferrate(III); potassium osmate(VI) dihydrate; In tert-butyl alcohol; at 20 ℃; for 7h;

Reference yield:

: 953817-79-3
phenyl 2,3,4-tri-O-benzyl-6-deoxy-6-fluoro-1-thio-α-D-mannopyranoside

: 1357098-65-7
3,4,5-tri-O-benzyl-7-deoxy-7-fluoro-D-glycero-α-D-lyxo-hept-2-ulopyranose

Guidance literature:: Multi-step reaction with 4 steps

1: N-Bromosuccinimide; water / acetone / 0.5 h / 20 °C

2: acetic anhydride / dimethyl sulfoxide / 24 h / 30 °C

3: toluene / 24 h / 60 °C / Inert atmosphere; Darkness

4: potassium carbonate; potassium hexacyanoferrate(III); water / potassium osmate(VI) dihydrate / tert-butyl alcohol / 7 h / 20 °C

With N-Bromosuccinimide; water; acetic anhydride; potassium carbonate; potassium hexacyanoferrate(III); potassium osmate(VI) dihydrate; In dimethyl sulfoxide; acetone; toluene; tert-butyl alcohol;

Reference yield:

: 1357098-63-5
2,3,4-tri-O-benzyl-6-deoxy-6-fluoro-D-mannono-1,5-lactone

: 1357098-65-7
3,4,5-tri-O-benzyl-7-deoxy-7-fluoro-D-glycero-α-D-lyxo-hept-2-ulopyranose

Guidance literature:: Multi-step reaction with 2 steps

1: toluene / 24 h / 60 °C / Inert atmosphere; Darkness

2: potassium carbonate; potassium hexacyanoferrate(III); water / potassium osmate(VI) dihydrate / tert-butyl alcohol / 7 h / 20 °C

With water; potassium carbonate; potassium hexacyanoferrate(III); potassium osmate(VI) dihydrate; In toluene; tert-butyl alcohol;