N-(5-benzoyl-2-phenyl-2H-1,2,3-triazol-4-yl)-2-cyanoacetamide

Base Information

• Chemical Name: N-(5-benzoyl-2-phenyl-2H-1,2,3-triazol-4-yl)-2-cyanoacetamide
• CAS No.: 1300047-83-9
• Molecular Formula: C₁₈H₁₃N₅O₂
• Molecular Weight: 331.334
• Mol file: 1300047-83-9.mol

Synonyms:N-(5-benzoyl-2-phenyl-2H-1,2,3-triazol-4-yl)-2-cyanoacetamide

Chemical Property of N-(5-benzoyl-2-phenyl-2H-1,2,3-triazol-4-yl)-2-cyanoacetamide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N-(5-benzoyl-2-phenyl-2H-1,2,3-triazol-4-yl)-2-cyanoacetamide

There total 1 articles about N-(5-benzoyl-2-phenyl-2H-1,2,3-triazol-4-yl)-2-cyanoacetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

(5-amino-2-phenyl-2H-1,2,3-triazol-4-yl)phenylmethanone (945016-91-1) + cyanoacetic acid (372-09-8) → N-(5-benzoyl-2-phenyl-2H-1,2,3-triazol-4-yl)-2-cyanoacetamide (1300047-83-9)

Guidance literature:

In acetic anhydride; at 85 - 100 ℃; for 0.0111111h; Microwave irradiation;

DOI:10.3390/molecules16053723

Reference yield: 87.0%

N-(5-benzoyl-2-phenyl-2H-1,2,3-triazol-4-yl)-2-cyanoacetamide (1300047-83-9) → 5-oxo-2,7-diphenyl-4,5-dihydro-2H-[1,2,3]triazolo[4,5-b]pyridine-6-carbonitrile (1300047-87-3)

Guidance literature:

With sodium acetate; In N,N-dimethyl-formamide; for 1h; Reflux;

DOI:10.3390/molecules16053723

upstream raw materials:

(5-amino-2-phenyl-2H-1,2,3-triazol-4-yl)phenylmethanone

cyanoacetic acid

Downstream raw materials:

5-oxo-2,7-diphenyl-4,5-dihydro-2H-[1,2,3]triazolo[4,5-b]pyridine-6-carbonitrile