6-benzyloxy-benzooxazole-3-carboxylic acid (3-trifluoromethyl-phenyl)-amide

Base Information

• Chemical Name: 6-benzyloxy-benzooxazole-3-carboxylic acid (3-trifluoromethyl-phenyl)-amide
• CAS No.: 890129-83-6
• Molecular Formula: C₂₂H₁₇F₃N₂O₃
• Molecular Weight: 414.384

Synonyms:6-benzyloxy-benzooxazole-3-carboxylic acid (3-trifluoromethyl-phenyl)-amide

Chemical Property of 6-benzyloxy-benzooxazole-3-carboxylic acid (3-trifluoromethyl-phenyl)-amide

Chemical Property:

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Technology Process of 6-benzyloxy-benzooxazole-3-carboxylic acid (3-trifluoromethyl-phenyl)-amide

There total 1 articles about 6-benzyloxy-benzooxazole-3-carboxylic acid (3-trifluoromethyl-phenyl)-amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-(4-benzyloxy-2-hydroxy-phenyl)-3-(3-trifluoromethyl-phenyl)-urea (890129-82-5) + 1,1-dibromomethane (74-95-3) → 6-benzyloxy-benzooxazole-3-carboxylic acid (3-trifluoromethyl-phenyl)-amide (890129-83-6)

Guidance literature:

With caesium carbonate; In N,N-dimethyl-formamide; at 20 ℃; for 10h;

Reference yield:

6-benzyloxy-benzooxazole-3-carboxylic acid (3-trifluoromethyl-phenyl)-amide (890129-83-6) → 6-hydroxy-benzooxazole-3-carboxylic acid (3-trifluoromethyl-phenyl)-amide (890129-84-7)

Guidance literature:

With hydrogen; palladium 10% on activated carbon; In tetrahydrofuran;

Reference yield:

6-benzyloxy-benzooxazole-3-carboxylic acid (3-trifluoromethyl-phenyl)-amide (890129-83-6) → β-hydroxy-benzooxazole-3-carboxylic acid (3-trifluoromethyl-phenyl)-amide

Guidance literature:

With hydrogen; palladium 10% on activated carbon; In tetrahydrofuran;

upstream raw materials:

1-(4-benzyloxy-2-hydroxy-phenyl)-3-(3-trifluoromethyl-phenyl)-urea

1,1-dibromomethane

Downstream raw materials:

6-hydroxy-benzooxazole-3-carboxylic acid (3-trifluoromethyl-phenyl)-amide

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