C₅₄H₇₈O₈Si₂

Base Information

Chemical Name:C₅₄H₇₈O₈Si₂
CAS No.:1310025-38-7
Molecular Formula:C₅₄H₇₈O₈Si₂
Molecular Weight:911.38
Hs Code.:

C<sub>54</sub>H<sub>78</sub>O<sub>8</sub>Si<sub>2</sub>

Synonyms:C₅₄H₇₈O₈Si₂

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Chemical Property of C₅₄H₇₈O₈Si₂

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Technology Process of C₅₄H₇₈O₈Si₂

There total 6 articles about C₅₄H₇₈O₈Si₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 994-30-9
triethylsilyl chloride

: 1310025-61-6
C₄₈H₆₄O₈Si

: 1310025-38-7
C₅₄H₇₈O₈Si₂

Guidance literature:: With 1H-imidazole; In dichloromethane; at 20 ℃; for 2h; Inert atmosphere;
DOI:10.1021/ja203034k

Reference yield:

: 1310025-34-3
C₃₄H₄₄O₅Si

: 1310025-38-7
C₅₄H₇₈O₈Si₂

Guidance literature:: Multi-step reaction with 5 steps

1.1: sodium hexamethyldisilazane / tetrahydrofuran; N,N-dimethyl-formamide / 0.03 h / Inert atmosphere; Cooling with ice

1.2: 0.33 h / 0 °C / Inert atmosphere

2.1: n-butyllithium; diisopropylamine / tetrahydrofuran; pentane / 0.23 h / -78 - 0 °C / Inert atmosphere

2.2: 0.77 h / -78 °C / Inert atmosphere

2.3: -78 °C

3.1: pyridinium p-toluenesulfonate / 3 h / 45 °C / Inert atmosphere

4.1: sodium tetrahydroborate; ethanol / 15 h / -15 °C / Inert atmosphere

5.1: 1H-imidazole / dichloromethane / 2 h / 20 °C / Inert atmosphere

With 1H-imidazole; sodium tetrahydroborate; n-butyllithium; ethanol; sodium hexamethyldisilazane; pyridinium p-toluenesulfonate; diisopropylamine; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; pentane;
DOI:10.1021/ja203034k

Reference yield:

: 1310025-37-6
C₄₈H₆₂O₈Si

: 1310025-38-7
C₅₄H₇₈O₈Si₂

Guidance literature:: Multi-step reaction with 2 steps

1: sodium tetrahydroborate; ethanol / 15 h / -15 °C / Inert atmosphere

2: 1H-imidazole / dichloromethane / 2 h / 20 °C / Inert atmosphere

With 1H-imidazole; sodium tetrahydroborate; ethanol; In dichloromethane;
DOI:10.1021/ja203034k