Phenyl 6,7-Dimethoxy-1-(3-pentylidene)-1,2,3,4-tetrahydroisoquinoline-2-carboxylate

Base Information

Chemical Name:Phenyl 6,7-Dimethoxy-1-(3-pentylidene)-1,2,3,4-tetrahydroisoquinoline-2-carboxylate
CAS No.:128425-88-7
Molecular Formula:C₂₃H₂₇NO₄
Molecular Weight:381.472
Hs Code.:

Synonyms:Phenyl 6,7-Dimethoxy-1-(3-pentylidene)-1,2,3,4-tetrahydroisoquinoline-2-carboxylate

Suppliers and Price of Phenyl 6,7-Dimethoxy-1-(3-pentylidene)-1,2,3,4-tetrahydroisoquinoline-2-carboxylate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Phenyl 6,7-Dimethoxy-1-(3-pentylidene)-1,2,3,4-tetrahydroisoquinoline-2-carboxylate

Chemical Property:

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Technology Process of Phenyl 6,7-Dimethoxy-1-(3-pentylidene)-1,2,3,4-tetrahydroisoquinoline-2-carboxylate

There total 1 articles about Phenyl 6,7-Dimethoxy-1-(3-pentylidene)-1,2,3,4-tetrahydroisoquinoline-2-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 128425-87-6
6,7-Dimethoxy-1-(3-pentyl)-3,4-dihydroisoquinoline

: 1885-14-9
phenyl chloroformate

: 128425-88-7
Phenyl 6,7-Dimethoxy-1-(3-pentylidene)-1,2,3,4-tetrahydroisoquinoline-2-carboxylate

Guidance literature:: With triethylamine; In dichloromethane; benzene; Heating;

Reference yield:

: 128425-88-7
Phenyl 6,7-Dimethoxy-1-(3-pentylidene)-1,2,3,4-tetrahydroisoquinoline-2-carboxylate

: 128425-92-3
1,1-Diethyl-1,5,6,10b-tetrahydro-8,9-dimethoxy-3H-oxazolo<4,3-a>isoquinolin-3-one

Guidance literature:: Multi-step reaction with 2 steps

1: 80 percent / Pb(OAc)4, glac. acetic acid / 0.5 h

2: 90 percent / sodium cyanoborohydride, glacial acetic acid

With lead(IV) acetate; sodium cyanoborohydride; acetic acid;