(1,2:4,6-Di-O-benzyliden-α-D-glucopyranose-3)-(1,2:3,5-di-O-benzyliden-α-D-glucofuranose-6)-natriumphosphat

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Chemical Name:(1,2:4,6-Di-O-benzyliden-α-D-glucopyranose-3)-(1,2:3,5-di-O-benzyliden-α-D-glucofuranose-6)-natriumphosphat
CAS No.:112104-99-1
Molecular Formula:C₄₀H₃₈O₁₄P*Na
Molecular Weight:796.697
Hs Code.:

Synonyms:(1,2:4,6-Di-O-benzyliden-α-D-glucopyranose-3)-(1,2:3,5-di-O-benzyliden-α-D-glucofuranose-6)-natriumphosphat

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Chemical Property of (1,2:4,6-Di-O-benzyliden-α-D-glucopyranose-3)-(1,2:3,5-di-O-benzyliden-α-D-glucofuranose-6)-natriumphosphat

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Technology Process of (1,2:4,6-Di-O-benzyliden-α-D-glucopyranose-3)-(1,2:3,5-di-O-benzyliden-α-D-glucofuranose-6)-natriumphosphat

There total 3 articles about (1,2:4,6-Di-O-benzyliden-α-D-glucopyranose-3)-(1,2:3,5-di-O-benzyliden-α-D-glucofuranose-6)-natriumphosphat which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

: 112104-86-6
(1,2:4,6-Di-O-benzyliden-α-D-glucopyranose-3)-(1,2:3,5-di-O-benzyliden-α-D-glucofuranose-6)-(2-chlorphenyl)-phosphat

: 112104-99-1
(1,2:4,6-Di-O-benzyliden-α-D-glucopyranose-3)-(1,2:3,5-di-O-benzyliden-α-D-glucofuranose-6)-natriumphosphat

Guidance literature:: With sodium hydroxide; 2-hydroxyiminomethyl-pyridine; 1,1,3,3-tetramethylguanidine; In 1,4-dioxane; water; for 72h; Ambient temperature;
DOI:10.1016/0008-6215(86)84003-4

Reference yield:

: 22164-08-5
1,2:3,5-Di-O-benzyliden-α-D-glucofuranose

: 112104-99-1
(1,2:4,6-Di-O-benzyliden-α-D-glucopyranose-3)-(1,2:3,5-di-O-benzyliden-α-D-glucofuranose-6)-natriumphosphat

Guidance literature:: Multi-step reaction with 2 steps

1: 47 percent / 1-Mesitylensulfonsaeure-<1H>-3-nitrotriazol / pyridine / 0.75 h / Ambient temperature

2: 58 percent / Pyridin-2-carbaldoxim, Tetramethylguanidine, NaOH / dioxane; H₂O / 72 h / Ambient temperature

With sodium hydroxide; 2-hydroxyiminomethyl-pyridine; 1,1,3,3-tetramethylguanidine; 1-Mesitylensulfonsaeure-<1H>-3-nitrotriazol; In 1,4-dioxane; pyridine; water;
DOI:10.1016/0008-6215(86)84003-4

Reference yield:

: 112104-81-1,112105-03-0
(1,2:4,6-Di-O-benzyliden-α-D-glucopyranose-3)-(2-chlorphenyl)-(triethylammonium)-phosphat

: 112104-99-1
(1,2:4,6-Di-O-benzyliden-α-D-glucopyranose-3)-(1,2:3,5-di-O-benzyliden-α-D-glucofuranose-6)-natriumphosphat

Guidance literature:: Multi-step reaction with 2 steps

1: 47 percent / 1-Mesitylensulfonsaeure-<1H>-3-nitrotriazol / pyridine / 0.75 h / Ambient temperature

2: 58 percent / Pyridin-2-carbaldoxim, Tetramethylguanidine, NaOH / dioxane; H₂O / 72 h / Ambient temperature

With sodium hydroxide; 2-hydroxyiminomethyl-pyridine; 1,1,3,3-tetramethylguanidine; 1-Mesitylensulfonsaeure-<1H>-3-nitrotriazol; In 1,4-dioxane; pyridine; water;
DOI:10.1016/0008-6215(86)84003-4