(1,2:4,6-Di-O-benzyliden-α-D-glucopyranose-3)-(1,2:3,5-di-O-benzyliden-α-D-glucofuranose-6)-(2-chlorphenyl)-phosphat

Base Information

Chemical Name:(1,2:4,6-Di-O-benzyliden-α-D-glucopyranose-3)-(1,2:3,5-di-O-benzyliden-α-D-glucofuranose-6)-(2-chlorphenyl)-phosphat
CAS No.:112104-86-6
Molecular Formula:C₄₆H₄₂ClO₁₄P
Molecular Weight:885.258
Hs Code.:

Synonyms:(1,2:4,6-Di-O-benzyliden-α-D-glucopyranose-3)-(1,2:3,5-di-O-benzyliden-α-D-glucofuranose-6)-(2-chlorphenyl)-phosphat

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Chemical Property of (1,2:4,6-Di-O-benzyliden-α-D-glucopyranose-3)-(1,2:3,5-di-O-benzyliden-α-D-glucofuranose-6)-(2-chlorphenyl)-phosphat

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Technology Process of (1,2:4,6-Di-O-benzyliden-α-D-glucopyranose-3)-(1,2:3,5-di-O-benzyliden-α-D-glucofuranose-6)-(2-chlorphenyl)-phosphat

There total 2 articles about (1,2:4,6-Di-O-benzyliden-α-D-glucopyranose-3)-(1,2:3,5-di-O-benzyliden-α-D-glucofuranose-6)-(2-chlorphenyl)-phosphat which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 47.0%

: 22164-08-5
1,2:3,5-Di-O-benzyliden-α-D-glucofuranose

: 112104-81-1,112105-03-0
(1,2:4,6-Di-O-benzyliden-α-D-glucopyranose-3)-(2-chlorphenyl)-(triethylammonium)-phosphat

: 112104-86-6
(1,2:4,6-Di-O-benzyliden-α-D-glucopyranose-3)-(1,2:3,5-di-O-benzyliden-α-D-glucofuranose-6)-(2-chlorphenyl)-phosphat

Guidance literature:: With 1-Mesitylensulfonsaeure-<1H>-3-nitrotriazol; In pyridine; for 0.75h; Ambient temperature;
DOI:10.1016/0008-6215(86)84003-4

Reference yield:

: 15074-54-1
2-chlorophenyl dichlorophosphate

: 112104-86-6
(1,2:4,6-Di-O-benzyliden-α-D-glucopyranose-3)-(1,2:3,5-di-O-benzyliden-α-D-glucofuranose-6)-(2-chlorphenyl)-phosphat

Guidance literature:: Multi-step reaction with 2 steps

1: 80 percent / 1,2,4-Triazol / pyridine / 0.5 h

2: 47 percent / 1-Mesitylensulfonsaeure-<1H>-3-nitrotriazol / pyridine / 0.75 h / Ambient temperature

With 1,2,4-Triazole; 1-Mesitylensulfonsaeure-<1H>-3-nitrotriazol; In pyridine;
DOI:10.1016/0008-6215(86)84003-4

Reference yield: 58.0%

: 112104-86-6
(1,2:4,6-Di-O-benzyliden-α-D-glucopyranose-3)-(1,2:3,5-di-O-benzyliden-α-D-glucofuranose-6)-(2-chlorphenyl)-phosphat

: 112104-99-1
(1,2:4,6-Di-O-benzyliden-α-D-glucopyranose-3)-(1,2:3,5-di-O-benzyliden-α-D-glucofuranose-6)-natriumphosphat

Guidance literature:: With sodium hydroxide; 2-hydroxyiminomethyl-pyridine; 1,1,3,3-tetramethylguanidine; In 1,4-dioxane; water; for 72h; Ambient temperature;
DOI:10.1016/0008-6215(86)84003-4